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A kind of non-silicon oil agent/silicon-containing oil agent compounded carbon fiber oil agent and preparation method thereof

A technology of carbon fiber and silicone oil, applied in the direction of carbon fiber, fiber treatment, carboxylic acid halide preparation, etc., can solve the problem of insufficient heat resistance, and achieve improved heat resistance, good heat resistance and lubricity, and improved heat resistance. sexual effect

Active Publication Date: 2017-03-08
新元化学(山东)股份有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] In view of the deficiencies of the prior art, the present invention provides a non-silicon oil / silicon-containing oil compounded carbon fiber oil and its preparation method, which solves the problem of insufficient heat resistance of the current oil for the preparation of high-performance carbon fibers. And it can be used in combination with non-silicone oil agent and silicone oil agent to meet the preparation needs of high-performance carbon fibers in different processes and improve the quality of carbon fibers

Method used

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  • A kind of non-silicon oil agent/silicon-containing oil agent compounded carbon fiber oil agent and preparation method thereof
  • A kind of non-silicon oil agent/silicon-containing oil agent compounded carbon fiber oil agent and preparation method thereof
  • A kind of non-silicon oil agent/silicon-containing oil agent compounded carbon fiber oil agent and preparation method thereof

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Embodiment 1～5

[0055] A non-silicon oil agent / silicon-containing oil compound compounded carbon fiber oil, which is obtained by compounding a non-silicon oil agent and a silicon-containing oil agent;

[0056] The non-silicone oil agent comprises 100 parts by mass of compound A, 1-5 parts by mass of antioxidant and 20-30 parts by mass of surfactant; said compound A has a structure shown in formula (I):

[0057]

[0058] In formula (I), a=0~3, b=6~10;

[0059] The silicone-containing oil agent includes 100 parts by mass of side chain aminopropyl modified silicone oil, 3-10 parts by mass of substance B and 20-30 parts by mass of surfactant; the substance B has the structure shown in formula (II) :

[0060]

[0061] In formula (II), z=2-5.

[0062] The preparation method of compound A:

[0063] (1) Add 103.5g of terephthalamide and 300mL of xylene into a 1000mL four-necked flask, stir and raise the temperature to 90°C, add 163.5g of lauroyl chloride dropwise, and pass in N 2 , take awa...

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Abstract

The invention relates to a carbon fiber oiling agent with a non-silicon oiling agent and a silicon-containing oiling agent compounded for use and a preparation method of the carbon fiber oiling agent. The carbon fiber oiling agent is obtained by compounding the non-silicon oiling agent and the silicon-containing oiling agent. The non-silicon oiling agent is prepared from, by mass, 100 parts of high heat-resisting compound A, 1-5 parts of antioxygen and 20-30 parts of surface active agent. The silicon-containing oiling agent is prepared from, by mass, 100 parts of side chain aminopropyl modified silicon oil, 3-10 parts of matter B and 20-30 parts of surface active agent. The carbon fiber oiling agent solves the problem of insufficient heat resistance of an existing oiling agent in the high-performance carbon fiber preparation process, and the non-silicon oiling agent and the silicon-containing oiling agent are matched for use, the preparation need of high-performance carbon fibers under different technological conditions can be met, so that the quality of the carbon fibers is improved.

Description

technical field [0001] The invention relates to an oil agent and a preparation method thereof, in particular to a carbon fiber oil agent compounded with a non-silicon oil agent / silicon-containing oil agent and a preparation method thereof, and belongs to the technical field of oil agents. Background technique [0002] Polyacrylonitrile-based carbon fiber (hereinafter referred to as carbon fiber) is an inorganic polymer fiber with a carbon content higher than 90%. It is the main reinforcing fiber for advanced composite materials. It has the characteristics of high strength, low density, no creep, and corrosion resistance. Widely used in aerospace, national defense, automobile, wind power, construction and other industries. The main preparation process of carbon fiber includes steps such as spinning, coagulation, drawing, oiling, steam drawing, setting, winding, pre-oxidation, low-temperature carbonization, high-temperature carbonization, etc. The oil agent is used in the oili...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M15/507D06M15/643D06M15/65D06M13/224D06M13/152D06M13/463D06M15/53C08G77/26C08G63/191C08G77/38C08G77/12C07C69/40C07C67/14C07F7/08D06M101/40
Inventor 解乐福田志钢杨燕张殿松解承钢
Owner 新元化学(山东)股份有限公司
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