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Method for preparing common vladimiria root and fructus amomi and six-monarch drug preparation

A preparation method and preparation technology, which are applied in the field of preparation of Xiangsha Liujun preparation, can solve the problems that it is difficult to measure, the clinical efficacy of Xiangsha Liujun preparation is not ideal, etc., and achieves easy detection, remarkable medicinal effect, and improved medicinal effect. Effect

Inactive Publication Date: 2016-05-04
GUIZHOU BAIHUA PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the inventor found in the course of research that in the Xiangshaliujun preparation made by the existing extraction process, the active ingredient of woody aromatic lactone is not easy to be detected, which makes the clinical efficacy of the Xiangshaliujun preparation not ideal enough.

Method used

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  • Method for preparing common vladimiria root and fructus amomi and six-monarch drug preparation
  • Method for preparing common vladimiria root and fructus amomi and six-monarch drug preparation
  • Method for preparing common vladimiria root and fructus amomi and six-monarch drug preparation

Examples

Experimental program
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Effect test

Embodiment 1

[0078] Recipe: Woody Fragrant 70g, Amomum 80g, Codonopsis 100g, Stir-fried Atractylodes macrocephala 200g, Poria cocos 200g, Zhilicorice 70g, Tangerine peel 80g, Jiang Pinellia 100g and accessories.

[0079] Process: take the woody incense, extract the volatile oil by steam distillation, and set aside; add 10 times the amount of water to the medicinal residue to extract twice, 2 hours each time, filter, combine the filtrate, concentrate it into a concentrated solution, and set aside; add 8 times the amount of 60 to the filter residue % ethanol solution, reflux extraction for 3 times, each time for 1h, filter, combine the filtrate, recover ethanol, and obtain the alcohol extract, combine the alcohol extract with the above water extract, and concentrate to 50-60°C when the relative density is 1.10-1.20 extract, dry and pulverize to obtain the dry paste powder of Muxiang, which is set aside; take Codonopsis pilosula, add 10 times of water to decoct 3 times, each time for 2 hours, ...

Embodiment 2

[0083] Recipe: Woody Fragrant 70g, Amomum 80g, Codonopsis 100g, Stir-fried Atractylodes macrocephala 200g, Poria cocos 200g, Zhilicorice 70g, Tangerine peel 80g, Jiang Pinellia 100g and accessories.

[0084] Process: Take the woody incense, distill it with water to extract the volatile oil, set aside; add 10 times the amount of water to the medicinal residue to extract twice, 2 hours each time, filter, combine the filtrate, concentrate it into a concentrated solution, and set aside; add 8 times the amount of 60 to the filter residue % ethanol solution, reflux extraction for 3 times, 1 hour each time, filter, combine the filtrate, recover ethanol, and obtain the alcohol extract, combine the alcohol extract with the above water extract, and concentrate to 50-60°C when the relative density is 1.10-1.20 extract, dry and pulverize to obtain the dry paste powder of Muxiang, which is set aside; take Codonopsis pilosula, add 10 times of water to decoct 3 times, each time for 2 hours, f...

Embodiment 3

[0088] Recipe: Woody Fragrant 70g, Amomum 80g, Codonopsis 100g, Stir-fried Atractylodes macrocephala 200g, Poria cocos 200g, Zhilicorice 70g, Tangerine peel 80g, Jiang Pinellia 100g and accessories.

[0089] Process: Take the woody incense, distill it with water to extract the volatile oil, set aside; add 10 times the amount of water to the medicinal residue to extract twice, 2 hours each time, filter, combine the filtrate, concentrate it into a concentrated solution, and set aside; add 8 times the amount of 60 to the filter residue % ethanol solution, reflux extraction for 3 times, each time for 1h, filter, combine the filtrate, recover ethanol, and obtain the alcohol extract, combine the alcohol extract with the above water extract, and concentrate to 50-60°C when the relative density is 1.10-1.20 extract, dry and pulverize to obtain the dry paste powder of Muxiang, which is set aside; take Codonopsis pilosula, add 10 times of water to decoct 3 times, each time for 2 hours, f...

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Abstract

The invention discloses a method for preparing a common vladimiria root and fructus amomi and six-monarch drug preparation. The common vladimiria root and fructus amomi and six-monarch drug preparation is mainly prepared from common vladimiria root, fructus amomi, radix codonopsis, fried rhizoma atractylodis macrocephalae, poria cocos, radix glycyrrhizae preparata, tangerine peel and ginger processed pinellia. Through the method disclosed by the invention, according to properties of all drugs in a prescription of the common vladimiria root and fructus amomi and six-monarch drug preparation, and functions of the drugs in the formula, a specific process for preparing the common vladimiria root and fructus amomi and six-monarch drug preparation and parameters are improved, so that effective component costunolide of common vladimiria root can be easily measured, and the content of measured costunolide is high, therefore the preparation is more refined, has a more obvious drug effect and has a good clinical effect.

Description

technical field [0001] The invention belongs to the field of traditional Chinese medicines, and in particular relates to a preparation method of Xiangsha Liujun preparation. Background technique [0002] Extraction of traditional Chinese medicine is a commonly used method in traditional Chinese medicine pharmacy. The chemical composition of traditional Chinese medicine is extremely complex, and it is necessary to extract the active ingredients of traditional Chinese medicine that are effective for the human body from the complex mixture. to improve efficacy. [0003] Xiangsha Liujun preparation is mainly made of Codonopsis pilosula, fried citrus aurantium, woody fragrance, fried malt and fried hawthorn; it has the effect of nourishing qi, strengthening spleen and harmonizing stomach. For spleen deficiency and Qi stagnation, indigestion, abdominal fullness, loose stool and other diseases. [0004] In the prior art, the preparation of Xiangsha Liujun is made in the following...

Claims

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Application Information

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IPC IPC(8): A61K36/9064A61P1/14A61P1/12
CPCA61K36/285A61K9/1652A61K9/2059A61K36/076A61K36/284A61K36/344A61K36/484A61K36/752A61K36/8888A61K36/9064A61K2236/331A61K2236/333A61K2236/39A61K2236/51A61K2236/53
Inventor 黄文荣马静
Owner GUIZHOU BAIHUA PHARMA
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