A kind of high-transparency optical film and its preparation method
An erasing film and high-transparency technology, applied in optics, optical components, instruments, etc., can solve problems such as deterioration of electronic components, easy penetration of water vapor, and high cost of coating films, so as to improve flexibility and improve vision effect, the effect of improving the refractive index
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Embodiment 1
[0032] Preparation of IM layer coating solution: 100 parts by mass of dipentaerythritol pentaacrylate, 20 parts by mass of zinc sulfide with a particle size of 0.08 μm, 30 parts by mass of calcium fluoride with a particle size of 0.01 μm, 100 parts by mass of zinc sulfide with a particle size of 0.3 μm Zinc oxide, use 100 parts by mass of propylene glycol monomethyl ether as a diluting solvent, then add 650 parts by mass of methyl ethyl ketone for dilution, and 0.5 parts by mass of 2-hydroxyl 2-methyl 1-phenylacetone to obtain a solid content of 25%. The IM layer coating solution.
[0033] Preparation of hard coating solution: 100 parts by mass of acrylic hardened resin coating solution, add 1 part by mass of trimethylchlorosiloxane, 50 parts by mass of toluene and 0.1 part by mass of benzophenone, and mix well to obtain the solid content It is 35.8% hardcoating solution.
[0034] Wherein the acrylic hardened resin coating solution is a mixture of 50 parts by mass of trimethy...
Embodiment 2
[0037] Prepare the IM layer coating solution: 100 parts by mass of dipentaerythritol tetraacrylate, 20 parts by mass of zinc sulfide (0.05 μm in particle size), 30 parts by mass of calcium fluoride (0.1 μm in particle size), 100 parts by mass of titanium oxide (0.2 μm in particle size μm), using 100 parts by mass of ethyl acetate as a diluting solvent, then adding 650 parts by mass of cyclohexanone for dilution and 1.0 parts by mass of diphenyl ethyl ketone, and mixing evenly to obtain an IM layer coating solution with a solid content of 25%.
[0038] Preparation of hard coating solution: 100 parts by mass of acrylate hard resin coating solution, add 3 parts by mass of trimethylchlorosiloxane, 30 parts by mass of cyclohexanone and 0.5 part by mass of methyl benzoylformate, mix After uniformity, a hardcoat coating solution with a solid content of 28.5% was obtained.
[0039] The acrylate hardening resin coating solution is a mixture of 32 parts by mass of dipentaerythritol pent...
Embodiment 3
[0042] Prepare the IM layer coating solution: get 100 parts by mass of dipentaerythritol hexaacrylate, 20 parts by mass of zinc sulfide (0.05 μm in particle size), 30 parts by mass of calcium fluoride (0.1 μm in particle size), 100 parts by mass of zirconia (particle size in 0.3 μm), 50 parts by mass of zinc oxide (particle size 0.2 μm), using 100 parts by mass of propylene glycol monomethyl ether as a dilution solvent, then adding 650 parts by mass of methyl ethyl ketone for dilution and 0.8 parts by mass of 2-hydroxyl 2-methyl ether Base 1-phenylacetone, after mixing evenly, the IM layer coating solution with a solid content of 28.6% was obtained.
[0043] Preparation of hard coating solution: 100 parts by mass of acrylic hardening resin coating solution, adding 5 parts by mass of trimethylchlorosiloxane, 15 parts by mass of methyl ethyl ketone and 0.3 parts by mass of methyl benzoylformate and mix uniformly to obtain a hardcoat coating solution with a solid content of 50.0%...
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