Fluorenyl triangular-prism-shaped organic cage compound, and preparation method and application of compound
A technology of triangular prism and organic cage is applied in the field of fluorenyl triangular prism-shaped organic cage compound and its preparation, which can solve the problems of complex and difficult preparation process of organic molecular cage compound, and achieves easy solution processing, low cost and regular structure. Effect
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[0036] Fluorenyl triangular prism organic cage compound, when W is C, Ar 1 is triphenylamine, Ar 2 When it is p-bromooctyloxybenzene, its structure is as follows:
[0037]
[0038] The key step of the preparation method of the above-mentioned fluorenyl triangular prism-shaped organic cage compound is to obtain the organic cage compound through Suzuki coupling reaction and acid-catalyzed Friedel-Crafts reaction ring closure. The specific reaction is as follows:
[0039]
[0040] Take the 100mL two-neck flask, magnet, and condenser out of the oven and assemble the instrument. Magnesium (0.41g, 17.03mmol) and a magneton were added to the reaction flask, sealed, vacuumed, drum N 2 . THF (8.6 mL) and p-bromooctyloxybenzene (4.4 g, 15.43 mmol) from which water had been removed were drawn into a syringe. Then a small amount of THF and p-bromooctyloxybenzene were added to the reaction flask. Heat the initiation with a heat gun while stirring, and the initiation is successf...
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