Low-field nuclear magnetic resonance multi-probe quantitative test system and method special for hydrate

A low-field nuclear magnetic resonance and test system technology, which is applied in the analysis by nuclear magnetic resonance, material analysis through resonance, and measurement devices, etc., can solve the problems of lack, complexity and failure of experimental test systems, and achieve accurate transverse relaxation rate Reliable, easy-to-use results

Pending Publication Date: 2018-03-16
QINGDAO INST OF MARINE GEOLOGY
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Problems solved by technology

However, the pore-scale behavior of hydrate-bearing sediments is more complex than that of conventional geotechnical materials, and the corresponding measurement experiments need to be carried out under low temperature and high pressure conditions, resulting in the existing low-field NMR measurements such as mercury porosimetry and dehumidification methods. The signal quantitative calibration method fails, and the low-field NMR quantitative test technology has encountered unprecedented challenges in the field of natural gas hydrate research, and the corresponding experimental test methods and supporting experimental test systems are still relatively scarce

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  • Low-field nuclear magnetic resonance multi-probe quantitative test system and method special for hydrate
  • Low-field nuclear magnetic resonance multi-probe quantitative test system and method special for hydrate
  • Low-field nuclear magnetic resonance multi-probe quantitative test system and method special for hydrate

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Embodiment 1

[0045] Example 1, a low-field nuclear magnetic resonance multi-probe quantitative test system for hydrates, including an industrial computer and a low-field nuclear magnetic resonance analyzer connected to the industrial computer, a temperature confining pressure control module and a pore fluid supply module, and a low-field nuclear magnetic resonance The analyzer is used for nuclear magnetic resonance relaxation spectrum analysis and imaging analysis of the test sample, and according to the actual test sequence, the low-field nuclear magnetic resonance analyzer is equipped with a normal temperature and pressure probe without confining pressure and a low temperature and high pressure probe without confining pressure and low-temperature and high-pressure probes with confining pressure, and three parallel test samples prepared by the same process are installed in the three probes. The size, quality and porosity of the three test samples are the same, and the length of the test sam...

Embodiment 2

[0056] Embodiment 2, based on the test system described above, the present invention also proposes a special low-field nuclear magnetic resonance multi-probe quantitative test method for hydrates, such as Figure 6 shown, including the following steps:

[0057] (1) Prepare parallel soil samples:

[0058] Using the same procedure to prepare three parallel soil samples, i.e. test samples, the three soil samples have the same size, the same mass and the same porosity, to ensure that the pore structure of the three soil samples is the same in a statistical sense;

[0059] (2) Probe measurement without confining pressure at normal temperature and pressure: analysis of pore structure of anhydrous soil samples;

[0060] Take a soil sample and place it in a probe without confining pressure at normal temperature and pressure. After distilling the saturated soil sample, install it on a low-field NMR analyzer. Run the low-field NMR analyzer to obtain the T2 distribution curve. The quali...

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Abstract

The invention discloses a low-field nuclear magnetic resonance multi-probe quantitative testing system and method for hydrates. The normal temperature and pressure probe, the temperature confining pressure control module, the pore fluid supply module and the industrial computer, through the combined use and structure of the low temperature and high pressure probe with confining pressure, the low temperature and high pressure probe without confining pressure and the normal temperature and pressure probe without confining pressure The improved design of the multi-probe method realizes the quantitative calibration of low-field NMR measurement signals of hydrate-containing sediments and the integrated research of the pore-scale behavior measurement and analysis of hydrate-containing sediments, which facilitates the pore-scale behavior of hydrate-containing sediments. The characteristic research lays the foundation for the exploration of the microcosmic mechanism of the basic physical parameters of hydrate-bearing sediments.

Description

technical field [0001] The invention belongs to the field of basic physical property testing of unconventional oil and gas reservoir engineering and geotechnical engineering, and specifically relates to a special low-field nuclear magnetic resonance multi-probe quantitative testing system and method for hydrates. Background technique [0002] Gas hydrate is widely distributed in deep ocean stratum environment and permafrost stratum environment in nature. It is rich in natural gas and is considered as an important potential alternative energy source. The dissociation of gas hydrates will weaken the reservoir strength and release a large amount of potent greenhouse gases, and it is also considered as a possible mechanism for inducing engineering geological disasters and global climate change. Therefore, natural gas hydrate has received extensive attention worldwide, and researchers from various countries have carried out a lot of research work from different angles, and on thi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N24/08
CPCG01N24/081
Inventor 刘昌岭刘乐乐孟庆国张准李承峰
Owner QINGDAO INST OF MARINE GEOLOGY
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