Abdomen warming patch and preparation method thereof
A technology of abdominal plasters and plasters, applied in the field of warming abdominal plasters and its preparation, can solve the problems of inconvenient use of moxibustion, inability of patients to move or work at the same time, inconvenient to carry, etc., so as to relieve and eliminate pain, and the process parameters are easy to use The effect of control and portability
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Embodiment 1
[0023] Take 10g mugwort leaves, 5g aconite, and 1g cinnamon. Add 10 times of water, carry out combined extraction with double extraction, extraction time is 2h, extract 3 times, collect the extract and volatile oil, wherein the extracted volatile oil is 0.1ml, set aside, the extract is concentrated to a ratio of medicine to liquid of 1.5:1, Precipitate with 80% ethanol, let it stand for 24 hours, separate, recover the ethanol from the alcohol precipitation solution until it has no alcohol smell, adjust the concentration of the concentrated solution to be equivalent to 0.47g / mL of crude drug; pass the pretreated D101 large Pore adsorption resin column for dynamic adsorption, first eluted with 2BV of pure water, then 9BV of 60% ethanol, the elution rate was 2BV / h, the water liquid was discarded, the alcohol eluate was collected, the ethanol was recovered and continued to dry to obtain Drug dry powder 0.92g; take pressure-sensitive adhesive 5g, absolute ethanol 4g, glycerin 0.6...
Embodiment 2
[0026] Take 8g of Artemisia argyi leaves, 4g of aconite, and 0.5g of cinnamon, add 10 times of water, and carry out combined extraction with double extraction. The extraction time is 2 hours, and the extraction is 3 times. The extract and volatile oil are collected, and the extracted volatile oil is 0.1ml. After the extract is concentrated to a ratio of 1.5:1 to the drug solution, it is precipitated with 80% ethanol, left to stand for 24 hours, and separated. The ethanol is recovered from the alcohol precipitation solution until it has no alcohol smell, and the concentration of the concentrated solution is adjusted to be equivalent to 0.47g / mL of the crude drug; at 2BV The flow rate per hour is dynamically adsorbed through the D101 macroporous adsorption resin column that has been pretreated. First, it is eluted with 2BV of pure water, and then 9BV of 60% ethanol. The elution rate is 2BV / h, and the water is discarded. Collect the alcohol eluent, recover the ethanol and continue...
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