Alkali metal cyanuric acid monohydrogen salt compound, its crystal, its preparation method and application
A compound, cyanuric acid technology, applied in the field of optoelectronic functional materials, can solve the problems such as insufficient use of advantages, parallel arrangement, wide band gap, etc.
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Embodiment 1
[0047] Preparation of KLi(HC) by aqueous solution method 3 N 3 o 3 )·2H 2 O, RbLi(HC 3 N 3 o 3 )·2H 2 O and RbNa(HC 3 N 3 o 3 )·2H 2 O single crystal
[0048]
[0049] The specific operation steps are as follows: after weighing the above-mentioned raw materials according to the above-mentioned dosage, put them into a 100ml beaker, put a magnet, put the beaker into a magnetic heating stirrer, heat up the beaker to 80°C while stirring, and then heat the beaker with 5 ℃ per hour cooling rate down to 40 ℃. After cooling, the sample was washed with acetone to obtain KLi(HC 3 N 3 o 3 )·2H 2 O single crystal.
[0050]
[0051] The specific operation steps are as follows: after weighing the above-mentioned raw materials according to the above-mentioned dosage, put them into a 100ml beaker, put a magnet, put the beaker into a magnetic heating stirrer, heat up the beaker to 80°C while stirring, and then heat the beaker with 5 ℃ per hour cooling rate down to 40 ℃. ...
Embodiment 2
[0055] Preparation of KLi(HC) by aqueous solution method 3 N 3 o 3 )·2H 2 O, RbLi(HC 3 N 3 o 3 )·2H 2 O and RbNa(HC 3 N 3 o 3 )·2H 2 O single crystal
[0056]
[0057] The specific operation steps are as follows: after the above-mentioned raw materials are weighed according to the above-mentioned dosage, put them into a 100ml beaker, put a magnet, put the beaker on a magnetic heating stirrer, heat the beaker to 80°C while stirring, and then use 1 ℃ per hour cooling rate down to 40 ℃. After cooling, the sample was washed with acetone to obtain KLi(HC 3 N 3 o 3 )·2H 2 O single crystal.
[0058]
[0059] The specific operation steps are as follows: after the above-mentioned raw materials are weighed according to the above-mentioned dosage, put them into a 100ml beaker, put a magnet, put the beaker on a magnetic heating stirrer, heat the beaker to 80°C while stirring, and then use 1 ℃ per hour cooling rate down to 40 ℃. After cooling, the sample was washed ...
Embodiment 3
[0063] The KLi(HC that embodiment 2 obtains 3 N 3 o 3 )·2H 2 O, RbLi(HC 3 N 3 o 3 )·2H 2 O and RbNa(HC 3 N3 o 3 )·2H 2 O crystal, processed cut, oriented, polished and placed figure 1 In the position of 3 in the device shown, at room temperature, Q-switched Nd:YAG laser is used as the input light source, and the incident wavelength is 1064nm. Obvious 532nm frequency-doubled green light output is observed, and the output intensity is about 2- 3 times. Specifically, KLi(HC 3 N 3 o 3 )·2H 2 The output intensity of O crystal is about 3 times that of KDP under the same conditions, RbLi(HC 3 N 3 o 3 )·2H 2 The output intensity of O crystal is about 2 times that of KDP under the same conditions, RbNa(HC 3 N 3 o 3 )·2H 2 The output intensity of O crystals is about 2 times that of KDP under the same conditions.
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