Fragrance materials
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example 1
Example Anhydrous Stick Compositions that Resist Habituation, Excluding Formula IV
[0320]
FormulaFormulaFormulaFormulaFormula IIIIIIIVFormula VVIInvisibleInvisibleInvisibleSoftSoftSoftSolidSolidSolidSolidSolidSolidAluminum24242426.526.526.5ZirconiumTrichlorohydrexGlycine PowderCyclopentasiloxaneQ.SQ.S.Q.S.Q.S.Q.S.Q.S.Dimethicone———555CO-1897 Stearyl141414———Alcohol NFHydrogenated3.853.853.85———Castor Oil MP80DeodorizedBehenyl Alcohol0.20.20.2———Tribehenin———4.54.54.5C 18-36 acid———1.1251.1251.125triglycerideC12-15 Alkyl9.59.55———BenzoatePPG-14 Butyl6.56.5—0.50.50.5EtherPhenyl3—3———TrimethiconeWhite Petrolatum3——333Mineral Oil1.01.01.0———Typical Perfume0.5——0.9——Marketed—————0.75PerfumePerfume Table 10.51.10.9—1.0—Beta-Cyclodextrin—3.0———3.0complexed withperfume Table 1Talc Imperial 2503.03.03.0———USPPolyacrylate——1.9———Microcapsuleloaded withperfume Table 1QS - indicates that this material is used to bring the total to 100%.
[0321]With the exception of Formula IV, the formulations defi...
example 2
Preformed Amine Reaction Product
[0338]The following ingredients are weighted off in a glass vial:[0339]50% of the perfume material comprising one or more off the perfumes claimed herein, for example, Table 1 perfumes A through G[0340]50% of Lupasol WF (CAS#09002-98-6) from BASF, is put at 60° C. in warm water bath for 1 hour before use. Mixing of the two ingredients is done by using the Ultra-Turrax T25 Basic equipment (from IKA) during 5 minutes. When the mixing is finished the sample is put in a warm water bath at 60° C. for ±12 hours. A homogenous, viscous material is obtained.
[0341]In the same way as described above different ratios between the components can be used:
Weight %Perfume Material4050607080Lupasol WF6050403020
example 3
84 wt % Core / 16 wt % Wall Melamine Formaldehyde (MF) Capsule (PAD Reservoir System
[0342]25 grams of butyl acrylate-acrylic acid copolymer emulsifier (Colloid C351, 25% solids, pka 4.5-4.7, (Kemira Chemicals, Inc. Kennesaw, Ga. U.S.A.) is dissolved and mixed in 200 grams deionized water. The pH of the solution is adjusted to pH of 4.0 with sodium hydroxide solution. 8 grams of partially methylated methylol melamine resin (Cymel 385, 80% solids, (Cytec Industries West Paterson, N.J., U.S.A.)) is added to the emulsifier solution. 200 grams of one or more off the perfumes claimed herein, for example, Table 1 perfumes A through G is added to the previous mixture under mechanical agitation and the temperature is raised to 50° C. After mixing at higher speed until a stable emulsion is obtained, the second solution and 4 grams of sodium sulfate salt are added to the emulsion. This second solution contains 10 grams of butyl acrylate-acrylic acid copolymer emulsifier (Colloid C351, 25% solids...
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