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51 results about "Glass Vial" patented technology

A glass container designed for use with parenteral drug products.

Application of Hemin@Zn-MOF material in catalytic oxidation

The invention discloses an application of a Hemin@Zn-MOF material in catalytic oxidation. The application comprises the following steps: S1, synthesizing Zn-MOF: S11, separately weighing Zn(NO3)2.6H2O(0.15g, 0.50 mmol), a ligand H3TATB (0.045g, 0.10 mmol) and an auxiliary ligand bpe (0.018 g, 0.10 mmol), placing the weighed reagents into a glass vial of 20 mL, adding 5 mL of dimethyl formamide (DMF) and 1 mL of H2O, and carrying out mixing and stirring; and S12, dropwise adding 0.7mL of a HNO3 solution (6 mol/L), carrying out stirring for 30 minutes, and then carrying out a reaction for 2 days in a drying oven at a temperature of 120 DEG C. The invention relates to the technical field of heme. According to the application of the Hemin@Zn-MOF material in catalytic oxidation, the hydrogen bond acting force between exposed free carboxyl of the two-dimensional Zn-MOF and carboxyl of the heme is utilized, the pi-pi acting force of the Zn-MOF ligand and a heme porphyrin ring is combined, and the combination between the Zn-MOF ligand and the heme is enhanced by the double acting force, so that chlorhematin is powerfully fixed on the material. In addition, the free carboxyl uniformly distributed in the Zn-MOF structure can easily achieve load uniformity of the heme. The Zn-MOF shows good stability in various solvents and pH (=1-10) environments, and catalytic application of the composite material is facilitated.
Owner:山西师范大学

Gas chromatographic analysis method for rapid determination of characteristic polymer material in mixture

ActiveCN104483396AEfficient separationAccurate determination of purityComponent separationGas liquid chromatographicN octane
The invention discloses a gas chromatographic analysis method for rapid determination of a characteristic polymer material in a mixture. The method comprises the following steps: firstly pouring a mixture powder to be measured into a reaction flask, adding an n-octane internal standard solution and an adipic acid solution; adding hydroiodic acid into the above reaction flask and sealing and weighing; putting the reaction flask into a drying oven, fully reacting, taking out the reaction flask, cooling, weighing, taking a supernatant as a test article for analysis; analyzing the test article by a gas chromatographic analysis method and acquiring data by starting a chromatographic acquisition computer system; and taking methyl iodide, ethyl iodide and isopropyl iodide compounds and transferring the compounds into a small glass bottle with a plug, adding 2ml of the n-octane internal standard solution and 2ml of the adipic acid solution, simultaneously carrying out gas chromatographic analysis, and calculating content of the characteristic polymer material in the mixture. The method provided by the invention has advantages of strong specificity, rapid analysis, strong resistance to interference and high sensitivity.
Owner:NOVAST LABORATORIES (CHINA) LTD

Atmospheric pressure photo ionization source device for detecting volatile organic compounds in water

The invention relates to a mass spectrometry instrument, in particular to an atmospheric pressure photo ionization source device for detecting volatile organic compounds in water. The device comprises a dynamic purging bubbling device and an atmospheric pressure photo ionization source. The dynamic purging bubbling device mainly comprises a small glass bottle, four capillary tubes, a bubbling bottle outlet and a constant-temperature water bath kettle. The atmospheric pressure photo ionization source comprises an ionization source cavity, a vacuum ultraviolet lamp, a repulsion electrode, a focusing electrode, a transmission electrode, a mass spectrum sample injection metal capillary tube, a reagent gas sample injection port, a high-humidity sample inlet and a supplementary gas inlet. And the high-humidity sample gas blown out of the bubbling bottle completely enters the atmospheric pressure photo ionization source. According to the invention, the detection stability is improved, and the influence of a matrix in water on sample detection is very small; the absorption of neutral molecules to photons and consumption of reagent ions are reduced; the ionization efficiency can be greatly improved by introducing the reagent gas. The designed atmospheric pressure photo ionization source can realize rapid and high-sensitivity detection of a high-humidity sample.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Method for simultaneously producing products on beer can production line and bottle (small bottle) production line sharing one sterilization machine

The invention provides a simultaneous production method for a beer can production line and a bottle production line (small bottles) which share a sterilizer. By a series of technical measures, the invention solves the problem in the traditional technique, that the cans and the small bottles with different sterilization temperature due to different materials can not use the same sterilizer during the production of the cans or the small bottles. The invention successfully uses the same sterilization temperature for sterilizing the glass small bottles (Pint) at an upper layer and the cans at a lower layer during the operation of the sterilizer. The invention realizes that the two different products can be produced in the same sterilizer and obtain the same sterilization quality. As to future beer manufacturers in China, methods used according to yield of the cans and the small bottles are as follows: when the yield of the small bottles is higher than the yield of the cans, not only the utilization rate of the energy in the sterilizer for producing the small bottles is enhanced by one time, but as to the cans, no production cost is consumed like using one invisible sterilizer; when the yield of the can is higher than the yield of the small bottles, the surpassing quantity can be solely produced by the can sterilizer; and the part of the yield of the can equal to the yield of the small bottle can be fulfilled by the invisible sterilizer; thus saving the cost of the electrothermal energy consumed by the sterilizer and strengthening the competitive power of an enterprise.
Owner:张学军

An atmospheric pressure photoionization source device for the detection of volatile organic compounds in water

The invention relates to a mass spectrometer analysis instrument, in particular to an atmospheric pressure photoionization source device for detecting volatile organic compounds in water. It includes two parts: a dynamic purging and bubbling device and an atmospheric pressure photoionization source. The dynamic purging and bubbling device mainly includes a glass vial, four capillaries, the outlet of the bubbling bottle, and a constant temperature water bath. Atmospheric pressure photoionization source includes ionization source cavity, vacuum ultraviolet lamp, repelling electrode, focusing electrode, transmission electrode, mass spectrometry sampling metal capillary, reagent gas inlet, high humidity sample inlet and make-up gas inlet. All the high-humidity sample gas purged from the bubble bottle enters the atmospheric pressure photoionization source. The invention improves the stability of detection, and the matrix in water has little influence on sample detection; the absorption of photons by neutral molecules and the consumption of reagent ions are reduced; the introduction of reagent gas can greatly improve the ionization efficiency. The designed atmospheric pressure photoionization source can realize rapid and highly sensitive detection of high-humidity samples.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

A zinc-based metal-organic framework with selective fluorescence recognition for acetylacetone and its preparation method

The invention relates to a zinc-based metal organic framework with a selective fluorescent recognition function on acetylacetone and a preparation method thereof. A chemical formula is C80H48N8O12Zn3;a crystal is crystallized in a monoclinic system; lattice parameters are as follows: a is equal to 18.96 angstroms, b is equal to 11.21 angstroms, c is equal to 36.62 angstroms, alpha is equal to 90degrees, beta is equal to 100.91 degrees and gamma is equal to 90 degrees. The invention further provides the preparation method of the zinc-based metal organic framework; the preparation method comprises the following steps: adding zinc nitrate hexahydrate, 1,3-bis(benzimidazole-1-yl)benzene, 1,4-naphthalic acid, N,N-dimethylformamide and ethanol into a small glass bottle; carrying out ultrasonictreatment to uniformly mix the materials; raising the temperature of a mixture and reacting for 65 to 80 h; cooling to obtain a colorless block-shaped crystal; collecting the crystal and washing withethanol; after drying in the air, obtaining the zinc-based metal organic framework. According to the preparation method provided by the invention, a new direction is provided for preparation of a light-emitting metal organic framework material based on a relatively strong coordination capability of divalent zinc ions and cooperative coordination of two organic ligands; the zinc-based metal organic framework can be used as a fluorescent material for recognizing small molecular organic matters and has potential application value in the fields of chemistry and materialogy.
Owner:JIANGXI UNIV OF SCI & TECH

Etalon effect suppression method and device for detection of residual oxygen in glass medicine bottles

The invention discloses an etalon effect suppression method and device for detecting the amount of residual oxygen in a glass medicine bottle. The method obtains the main transmitted light intensity after the laser penetrates the glass medicine bottle and the transmitted light intensity after two reflections, And convert it into the first current signal, obtain the transmitted light intensity after one reflection and the transmitted light intensity after three reflections when the laser penetrates the glass medicine bottle, and convert it into the second current signal, according to the first current signal and the second current signal, obtain the output current, extract the second harmonic current signal of the output current, and obtain the oxygen concentration according to the second harmonic current signal, which solves the problem caused by the beam interference generated by the wall of the glass medicine bottle in the prior art to the second harmonic The optical noise caused by the low detection accuracy of residual oxygen is a technical problem. By eliminating the noise in the second harmonic from the signal detection part, the etalon effect can be suppressed from the root, and the detection accuracy of oxygen concentration and the stability of the system are greatly improved. .
Owner:TRUKING TECH LTD
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