Aqueous concentrated herbicidal compositions containing glyphosate salts and dicamba salts
a technology of dicamba salt and concentrate composition, which is applied in the field of herbicidal concentrate compositions, can solve the problems of uncontrolled cell division and growth, abnormal leaf shape and venation, and slow uptake (i.e., absorption) of glyphosate by the plant foliar tissue, and achieve the effect of low volatility
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example 1
[0054]Various aqueous herbicidal concentrate compositions containing glyphosate salt and dicamba salt were prepared by adding the desired base (e.g., monoethanolamine (MEA), isopropylamine (IPA) or potassium hydroxide) to stock glyphosate salt solutions. Salt solutions of dicamba (e.g., diglycolamine (DGA), MEA, and K salts) were added to the glyphosate salt solutions to the desired acid equivalent weight ratio (e.g., glyphosate to dicamba weight ratios of 3:1, 2:1, or 1.5:1).
[0055]The solutions which provided stable, compatible herbicidal concentrate compositions upon mixing are listed below in Table 1.
TABLE 1Weight ratio a.e.Total herbicideGlyphosateDicamba(Glyphosate / loadingsaltsaltDicamba)(g / l a.e.)MEADGA3:1480MEAMEA3:1480MEAK3:1480IPADGA3:1360IPAMEA3:1360IPAK3:1360KDGA3:1220KMEA3:180KK3:180MEADGA2:1480MEAMEA2:1480MEAK2:1480IPADGA2:1330IPAMEA2:1330KDGA2:1330KMEA2:1330MEADGA1.5:1 480MEAMEA1.5:1 480MEAK1.5:1 480
example 2
[0056]To evaluate whether surfactant(s) could be effectively incorporated into the aqueous herbicidal concentrate compositions of the present invention, several concentrate solutions containing MEA glyphosate and DGA dicamba and having a total herbicidal loading of approximately 480 g / l a.e. were prepared as described in Example 1, except various surfactants were combined the solution concentrates. The stability of the solutions was observed upon mixing and any precipitation or phase separation was noted. The stability of the solutions that appeared relatively homogeneous upon mixing was tested further by storing them at room temperature for 24 hours. Any precipitation or phase separate was noted after the 24 hour time period. Table 2 presents the results of these experiments.
TABLE 2Surfactants combined with concentrates containing approx.480 g / l a.e. of MEA glyphosate salt and DGA dicamba salt.WeightStableratio a.e.Surfactantconcentrate after(Glyphosate / (wt. % inCloud24 hours?Dicam...
example 3
[0058]To evaluate whether higher concentrations of surfactant(s) could be effectively incorporated into the aqueous herbicidal concentrate compositions of the present invention, concentrate solutions containing a 1.5:1 weight ratio of MEA glyphosate and DGA dicamba and having a total herbicidal loading of approximately 480 g / l a.e. were prepared in accordance with Example 1. Ethoquad C-12 dissolved in propylene glycol or diethylene glycol was then combined with the concentrates. The stability of the solutions was observed and any precipitation or phase separation was noted. Table 3 presents the results of these experiments.
TABLE 3StableEthoquad C-12concentrate(wt. % inCloudformed?solution)Solventpoint(Yes / No)7.5Diethylene>90°C.YesGlycol10Diethylene85°C.YesGlycol7.5Propylene>90°C.YesGlycol10Propylene—NoGlycol
[0059]The results show that stable, clear herbicidal concentrates containing surfactant 10 wt. % Ethoquad C-12 dissolved in diethylene glycol were successfully prepared. The conc...
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