Method for mixedly extracting red date and seabuckthorn fruit for preparing spices for cigarette

A technology of mixed extraction and tobacco flavors, applied in the directions of essential oils/spice, tobacco, application, etc., can solve the problems of harm to health, bring miscellaneous gas, pollute the environment, etc., to increase sweetness, reduce irritation, separate The effect of high concentration efficiency

Active Publication Date: 2009-07-01
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method has the following disadvantages: A, the solvent itself is toxic, pollutes the environment, and is harmful to human health; B, when the concentration of n-hexane or sherwood oil in the air is at 1-6ryo (calculated by volume), an explosion can occur; C. Compared with ethanol solvent, the cost is higher
The applicant extracts jujubes alone for flavoring cigarettes, and the application in cigarettes has a certain effect, which can increase the aroma and sweetness of cigarettes, but it will bring miscellaneous odors and a slightly astringent aftertaste
The applicant extracts seabuckthorn alone and uses it in cigarettes. Seabuckthorn extract alone also has a certain effect in cigarettes, which can sweeten the smoke and improve the aftertaste, but it will cause irritation

Method used

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  • Method for mixedly extracting red date and seabuckthorn fruit for preparing spices for cigarette
  • Method for mixedly extracting red date and seabuckthorn fruit for preparing spices for cigarette
  • Method for mixedly extracting red date and seabuckthorn fruit for preparing spices for cigarette

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0053] Embodiment 1. Take by weighing 500g of red date dried fruit, 500g of seabuckthorn dried fruit (in this example, red date: seabuckthorn=1:1), put into the oven and dry at a constant temperature (50° C.) for 2 hours (moisture is controlled at about 5%). The red dates and sea buckthorn are crushed through a 20-mesh sieve. The amount of pure water added is twice that of jujube and seabuckthorn. After soaking overnight, extract and reflux in a water bath, and reflux twice for 4 hours each time. The extraction temperature is 80°C. After filtering, add 1 times the amount of 50% edible alcohol to the combined filtrate to settle overnight at low temperature, filter the next day and concentrate the filtrate to 18 bomm. The finished product of the mixture extract is a reddish-brown viscous liquid with sweet and sour fruity aroma, delicate fragrance and violet-like honey-sweet aroma.

Embodiment 2

[0054] Example 2. Weigh 340g of dried jujube fruit and 660g of seabuckthorn dried fruit (jujube: seabuckthorn ≈ 1:2), put them into an oven and dry them at a constant temperature (50°C) for 2 hours (moisture is controlled at about 5%), and dry the dried jujube, Seabuckthorn is crushed through a 60-mesh sieve. The amount of pure water added is 3 times that of jujube and seabuckthorn. After soaking overnight, extract and reflux in a water bath, reflux 3 times, each time for 6 hours, and the extraction temperature is 90°C. After filtering, add 2 times the amount of 75% edible alcohol to the combined filtrate to settle overnight at low temperature, and filter the next day and concentrate the filtrate to 19 bomm. The finished product of the mixture extract is bright red viscous liquid with sweet fruity and delicate fragrance.

Embodiment 3

[0055] Example 3. Weigh 660g of dried jujube and 340g of dried seabuckthorn (jujube: seabuckthorn ≈ 2:1), put them in an oven at constant temperature (50°C) and dry for 2 hours (moisture is controlled at about 5%), and dry red dates and seabuckthorn Crushed through 80 mesh sieve. The amount of pure water added is 4 times that of jujube and seabuckthorn. After soaking overnight, extract and reflux in a water bath, reflux 4 times, each time for 8 hours, and the extraction temperature is 100°C. After filtering, add 3 times the amount of 95% edible alcohol to the combined filtrate to settle overnight at low temperature, filter the next day and concentrate the filtrate to about 20 Bomido. The finished mixture extract is brown-red viscous liquid with sweet and sour fragrance and violet-like honey fragrance.

[0056] The following is the situation of carrying out the cigarette addition and smoking test on the mixed raw material extract of jujube and seabuckthorn in the above-mention...

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PUM

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Abstract

The invention discloses a method for preparing tobacco spice by mixing and extracting red dates and sea backthern, and belongs to the technical field of tobacco spice preparation in the cigarette industry. The method comprises: firstly, drying dried red date fruit and dried sea backthern fruit according to the proportion of 1-2:1-2 in an oven at a constant temperature (50 DEG C) for 2 hours (the moisture content is controlled to be approximately 5 percent), and crushing mixed materials through a 20 to 80 mesh sieve; secondly, taking 2 to 4 times of purified water as a solvent to soak the mixed materials over night, and performing extraction and reflux for 2 to 4 times and 4 to 8 hours each time, wherein the extraction temperature is between 80 and 100 DEG C; thirdly, adding filtrate into 1 to 3 times of 50 to 95 percent edible alcohol for low-temperature precipitation and filtration; and fourthly, concentrating the filtrate until the Baume degree is between 18 and 20, and obtaining the tobacco spice. Mixed extract of the method maintains the prior characteristics of respective extract, simultaneously generates novel fragrant substances, makes up for the defects of each other and sets off the advantages of each other. The method has the advantages of simple technology, small investment of production equipment, low operating cost and high separation and concentration efficiency.

Description

technical field [0001] The invention belongs to the technical field of preparation of flavors for tobacco in the cigarette industry, in particular to a method for preparing flavors for tobacco by mixing and extracting jujube and seabuckthorn. Background technique [0002] At present, the number of synthetic fragrances is increasing, but they are not as harmonious as natural fragrance ingredients and have rich aromas. Therefore, the application of natural flavors in the formulation of cigarette flavors is becoming more and more extensive, and the use of natural plant extracts as additives in cigarette flavoring has become one of the current focus and hot spots in the development of the tobacco industry. Some single natural plant extracts have better effects when added to tobacco, but some single natural extracts can also bring some negative effects while improving the smoking taste of cigarettes, such as increased irritation and poor aftertaste , There are residues in the mo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B15/28
Inventor 朱颖黄龙王珊赵国豪周湘肜霖董世良程书锋
Owner HUBEI CHINA TOBACCO IND
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