Poly glucosamine hexanedioic acid vinyl ester material for reducing content of phenol type substances
A technology of phenols and content, applied in the fields of food science, application, tobacco, etc., can solve the problems of increasing harmful components, complicated preparation process, influence of smoke taste, etc., to reduce harmful phenolic components, maintain internal quality, and avoid fragrance. The effect of component loss
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Embodiment 1
[0040] A 5 mg / mL aqueous solution of polyglucosamine vinyl adipate hydrochloride (solution A) and a 5 mg / mL aqueous solution of polygalactosyl acrylate (solution B) were prepared. Take 5.0g granular zeolite, mix it with 7.5ml solution B, stir evenly, and let stand at 15°C for 1h. Filter and bake all the solids at 60°C for 72h. The obtained solid was mixed with 10 mL of solution A, stirred evenly, and allowed to stand at 30° C. for 1 h. Filtrate and dry the filtered solid at 75°C for 50 hours to obtain a dry solid, that is, to complete one self-assembly, and then treat the dry solid with solution B and solution A for 10 times according to the above method to obtain 22 monolayers, The outermost layer is the above-mentioned polyglucosamine vinyl adipate hydrochloride hydrophilic polycation to obtain a composite material with high water retention, and the weight percentage of the polycation loaded in the composite material is 5%. In the infrared spectrum of the composite materia...
Embodiment 2
[0047] Dissolve polyglucosamine vinyl adipate hydrochloride in water to prepare an aqueous solution of 5 mg / mL polyglucosamine vinyl adipate hydrochloride (solution A) and an aqueous solution of 3 mg / mL sodium alginate (solution B) . Take 5.0g of powdered silica gel, mix it with 7.5ml of solution B, stir evenly, and let stand at 25°C for 3h. Filter and bake all the solids at 60°C for 72h. The obtained solid was mixed with 5 mL of solution A, stirred evenly, and allowed to stand at 25° C. for 1 h. Filtrate and dry the filtered solid at 75°C for 50 hours to obtain a dry solid, that is, to complete one self-assembly, and then treat the dry solid with solution B and solution A for 6 times according to the above method to obtain 8 monolayers, The outermost layer is the above-mentioned polyglucosamine vinyl adipate hydrochloride hydrophilic polycation to obtain a composite material with high water retention, and the weight percentage of the polycation loaded in the composite mater...
Embodiment 3
[0054] Polyglucosamine vinyl adipate hydrochloride was dissolved in water to prepare an aqueous solution of 0.2mg / mL polyglucosamine vinyl adipate hydrochloride (solution A) and an aqueous solution of 6mg / mL carboxymethyl chitosan (Solution B). Take 5.0g granular macroporous adsorption resin, mix it with 4ml solution B, stir evenly, and let stand at 15°C for 2h. Filter and bake all the solids at 60°C for 48h. The obtained solid was mixed with 10 mL of solution A, stirred evenly, and allowed to stand at 20° C. for 2 h. Filtrate and dry the filtered solid at 75°C for 50 hours to obtain a dry solid, that is, to complete one self-assembly, and then treat the dry solid with solution B and solution A for 5 times according to the above method to obtain 12 monolayers, The outermost layer is the above-mentioned polyglucosamine vinyl adipate hydrochloride hydrophilic polycation to obtain a composite material with high water retention, and the weight percentage of the polycation loaded...
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