Detection method of tambac depression-alleviating pill as traditional Chinese medical preparation
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A technology of Chenxiang Shuyu pills and traditional Chinese medicine preparations, applied in the direction of testing pharmaceutical preparations, material inspection products, etc., to achieve the effect of improving quality control and accurate detection
Active Publication Date: 2012-02-29
津药达仁堂集团股份有限公司达仁堂制药厂
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[0004] The current quality standard of Shenxiang Shuyu Pills has no specific identification method for each component, but only describes it from the microstructure, which is not conducive to the qualitative and quantitative detection of the drug , which brings great difficulties to the quality control of the drug. According to the search, there is currently no relevant patent on the quality control method of Chenxiang Shuyu Pills. The existing patents mainly focus on the important formula and method of Chenxiang Shuyu Pills
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[0037] Below in conjunction with the examples, the present invention is further described, the following examples are illustrative, not limiting, and the protection scope of the present invention cannot be limited by the following examples.
[0038] The quality control method of Chinese medicine preparation Chenxiang Shuyu pills, the steps of the method are:
[0039] (1) Characters and microscopic identification:
[0040] ①Character identification: The color of the original standard was described as a large brown honeyed pill. Since the production time of this product was 2004, the current appearance color is brown. On this basis, combined with the color of the core of the pellet, the color of this product is described as brown It is a large honeyed pill of brown to brown color, and its present properties are described as follows: This product is a large honeyed pill of brown to brown color; it tastes sweet and slightly bitter.
[0041] ②Observed under a microscope: the stone...
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Abstract
The invention relates to a quality control method of a tambac depression-alleviating pill as a traditional Chinese medical preparation. The method comprises the following steps of: firstly, carrying out character and microscopic identification; secondly, identifying whether a depression-alleviating pill prescription contains the contents of elecampane, fumitory and curcuma or not by adopting a film chromatography; and finally, measuring the magnolol content in the tambac depression-alleviating pill prescription by adopting a high-efficiency liquid-phase method and using magnolol and honokiol as reference substances. Based on an original standard of the tambac depression-alleviating pill, the microscopic identification methods of magnolia, rhizoma cyperi and astragalus in the prescription are added, the film identification methods of elecampane, fumitory and curcuma are added and a magnolia content measuring method is drawn up by using the magnolol and the honokiol as reference substances. The revised quality standard improves the pharmaceutical quality control and can ensure that traditional Chinese medicines are detected more accurately.
Description
technical field [0001] The invention belongs to the technical field of traditional Chinese medicines, and relates to a detection method of traditional Chinese medicines, in particular to a quality control method of Shenxiang Shuyu pills, a traditional Chinese medicine preparation. Background technique [0002] The ingredients of Chenxiang Shuyu Wan are woody, agarwood, tangerine peel, magnolia officinalis (made from ginger), cardamom, amomum, citrus aurantium (fried with bran), green skin (made from vinegar), Cyperus cyperi (made from vinegar), Corydalis (made from vinegar) ), bupleurum, turmeric, licorice, etc., crush the above thirteen traditional Chinese medicines into fine powder, mix well, sieve, add 170-190g of refined honey to each 100g of powder to make a large honeyed pill, that is, function and indications: Shu Qi whets the appetite, dispels stagnation and relieves pain, and is used for fullness of the chest and abdomen, stomach pain, vomiting of sour water, indig...
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