Spice for cigarettes and extracting method and application thereof

A technology of tobacco flavor and extraction method, applied in the field of tobacco flavoring, can solve the problems of resource consumption and the like, and achieve the effects of convenient application, simple operation and high extraction rate

Active Publication Date: 2012-10-03
CHINA TOBACCO HENAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, companies usually only extract the pectin and protein and apply them to the fields of medicine, beverages or animal husbandry, and the remaining substances are directly discarded, resulting in a huge waste of resources.

Method used

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  • Spice for cigarettes and extracting method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0012] Example 1: Add 500ml of silkworm excrement waste liquid after extracting chlorophyll and a little zeolite to one end of the simultaneous distillation extraction device, heat and boil with an electric heating mantle; the other end of the device (receiving end) contains 15mL of dichloromethane, heat it in a 60°C water bath, and distill and extract for 3 hours at the same time ; Use a rotary evaporator to evaporate the dichloromethane in the extract, and place the obtained spices in a brown bottle for sealed and refrigerated storage.

[0013] Dilute the obtained spices to 5% with absolute ethanol, spray 5g of diluent per 1000g of shredded tobacco (the amount of flavoring is 0.025% of the weight of shredded tobacco) evenly into the shredded tobacco, leave it at room temperature for 2 hours to absorb, and then smoke according to the normal process.

Embodiment 2

[0014] Example 2: Add 500ml of silkworm excrement waste liquid after extracting chlorophyll and a little zeolite to one end of the simultaneous distillation and extraction device, heat and boil with an electric heating mantle; 15mL of ethanol is contained in the receiving end of the device, heat with a water bath at 85°C, and distill and extract at the same time for 2 hours; evaporate with a rotary evaporator In addition to the ethanol in the extract, the obtained spices are placed in a brown bottle, sealed and refrigerated.

[0015] Dilute the obtained flavor with absolute ethanol to 10%, add 5g of diluent per 1000g of shredded tobacco (the amount of flavoring is 0.05% of the weight of shredded tobacco) and evenly spray it into shredded tobacco, leave it at room temperature for 2h to absorb, and then smoke according to the normal process.

Embodiment 3

[0016] Example 3: Add 500ml of silkworm excrement waste liquid after extracting chlorophyll and a little zeolite to one end of the simultaneous distillation and extraction device, heat and boil with an electric heating mantle; 20mL of acetone is contained in the receiving end of the device, heat with a 65°C water bath, and distill and extract at the same time for 5h; evaporate with a rotary evaporator In addition to the acetone in the extract, the obtained spices are placed in a brown bottle, sealed and refrigerated.

[0017] According to the ratio of 1000g shredded tobacco to 1g flavoring, the obtained flavoring is evenly sprayed into the shredded tobacco, left at room temperature for 2 hours for absorption, and then cigarettes are rolled according to the normal process.

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Abstract

The invention relates to spice for cigarettes and an extracting method and application of the spice, belonging to the technical field of tobacco processing, wherein the spice for the cigarettes is a solvent extract of silkworm excrement waste liquid obtained by extracting chlorophyll from the silkworm excrement; solvent is water, ethanol, acetone or methylene dichloride; the extracting method comprises the following steps: carrying out distillation and extraction to the silkworm excrement waste liquid obtained by extracting chlorophyll from the silkworm excrement for 2-5 hours by water, ethanol, acetone or methylene dichloride, and obtaining the spice after removing the solvent. According to the application of the spice for the cigarettes, the spice is used for flavoring the tobacco; dosage of the spice is 0.025-0.1% of tobacco shred weight; by dint of assay determination, the spice provided by the invention mainly contains twenty-odd aromatic matters such as irisone, furanone, isophorone, jasmine, phytol, phosphate, cyclohexanol and the like; these matters are added to cigarette tobacco shred, so that smoke sweet degree of the cigarettes can be improved obviously; sweet-back engender liquid of cigarette smoke is improved; smoke is softened; and aftertaste is improved. Simultaneously, the silkworm excrement waste liquid obtained by extracting chlorophyll from the silkworm excrement is changed from waste material into things of value; and resource is utilized fully.

Description

technical field [0001] The invention belongs to the technical field of tobacco flavoring, and relates to a flavor for tobacco extracted from industrial waste—silk excrement waste after chlorophyll extraction, and also relates to an extraction method and application of the flavor for tobacco. Background technique [0002] Silkworm excrement is a folk traditional Chinese medicine in my country. It is sweet, pungent, warm in nature, non-toxic, and has the functions of expelling wind and dampness, clearing heat and improving eyesight, promoting blood circulation and relieving pain. With the development of technology, silkworm excrement has become an important raw material for extracting chlorophyll in industry. However, after extracting chlorophyll, silkworm excrement waste liquid also contains a large amount of pectin, protein and other rich beneficial ingredients. At present, companies usually only extract the pectin and protein and apply them to the fields of medicine, bever...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B3/12
Inventor 杨志忠程向红韦凤杰田海英何景福董顺德张弘涛李禄成魏明杰赵伟民李文伟刘茂林
Owner CHINA TOBACCO HENAN IND
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