A detection method of Xianyu Capsules for the treatment of epileptic convulsions, infantile convulsions, and hemifacial spasms
A technique for the detection of convulsions in children, applied in the capsules for convulsions in children, hemifacial spasm, the detection of epilepsy convulsions, and epilepsy capsules. It can solve the problems of not formulating other ingredients and achieve good sample reproducibility , The effect of stable and controllable quality
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0050] Example 1 Prescription and preparation method of Xianyu Capsule
[0051] prescription:
[0052]
[0053]
[0054] Preparation method: The above sixteen flavors, stiff silkworm, and Liushenqu are crushed into fine powder, sieved, and set aside; the other fourteen flavors such as astragalus are boiled in water for three times, the first time is 2 hours, the second time is 1.5 hours, and the third time is 1 hour. hours, combined the decoction, filtered, the filtrate was concentrated under reduced pressure to a thick paste with a relative density of 1.36 (60°C), added the above fine powder, mixed evenly, dried in vacuum, crushed into a fine powder, and granulated with 80% ethanol in an appropriate amount. Dry at 70°C, pack into capsules, and make 1000 capsules.
[0055] Properties: This product is a hard capsule, the contents are brown to tan granules and powder; taste bitter.
Embodiment 2
[0056] Example 2 TLC Identification of Salvia Miltiorrhiza in Xianyu Capsules
[0057] 1. Test conditions: double-layer expansion cylinder (Shanghai Xinyi); silica gel G (for thin-layer chromatography, Qingdao Ocean Chemical Factory); homemade thin-layer plate with a thickness of 0.3mm. The rest of the reagents were analytically pure.
[0058] 2. Test procedure: Take 10 g of the capsule content prepared in Example 1, add 35 ml of 70% ethanol, heat and reflux for 30 minutes, filter, evaporate the filtrate to dry without ethanol smell, add 20 ml of water to dissolve, add 1mol / L hydrochloric acid to adjust the pH to 1 -2, then shake and extract with ethyl acetate 3 times, 10ml each time, combine the ethyl acetate solution, evaporate to dryness, add 2ml of methanol to dissolve, and use it as the test solution.
[0059] Another protocatechualdehyde reference substance, add methanol to make a solution containing 0.5mg per 1ml, as the reference substance solution.
[0060] Then t...
Embodiment 3
[0065] Example 3 TLC Identification of Salvia Miltiorrhiza in Xianyu Capsules
[0066] 1. Test conditions: double-layer expansion cylinder (Shanghai Xinyi); silica gel G (for thin-layer chromatography, Qingdao Ocean Chemical Factory); homemade thin-layer plate with a thickness of 0.3mm. The rest of the reagents were analytically pure.
[0067] 2. Test procedure: Take 10 g of the capsule content prepared in Example 1, add 35 ml of 70% ethanol, heat and reflux for 30 minutes, filter, evaporate the filtrate to dry without ethanol smell, add 20 ml of water to dissolve, add 1mol / L hydrochloric acid to adjust the pH to 1 -2, then shake and extract with ethyl acetate 3 times, 10ml each time, combine the ethyl acetate solution, evaporate to dryness, add 2ml of methanol to dissolve, and use it as the test solution.
[0068] Another protocatechualdehyde reference substance, add methanol to make a solution containing 0.5mg per 1ml, as the reference substance solution.
[0069] Then t...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com