Method for detecting residual tranquilizer medicines in meat product
A technology of meat products and tranquilizers, which is applied in the field of detection of drug residues in meat products, can solve the problems of expensive equipment and inability to be widely used in testing laboratories, and achieve the effects of simple operation, low detection cost and low detection limit
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[0045] The implementation of a method for detecting residues of various tranquilizers in meat products according to the present invention will be described in detail below with reference to the accompanying drawings.
[0046] The present invention is a method for detecting residues of various tranquilizers in meat products, and the following examples are provided:
[0047] 1. Testing instruments and equipment:
[0048] 7890A / 5975I GC-MS, capillary column DB-5MS (30m×0.25mm×0.25μm), C18 Solid phase extraction cartridge (3mL, 500mg), shaker, centrifuge, IKA vortex mixer.
[0049] 2. Reagents:
[0050] Standard products diazepam, oxazepam, estazolam, alprazolam, triazolam, phenobarbital, and promethazine, the contents of which are all greater than 99.0%. L of anhydrous methanol standard stock solution.
[0051] K at pH = 7.0 2 HPO 4 Buffer solution: Weigh a certain amount of K2HPO4 and dissolve it in distilled water, and adjust the pH to 7.0 with phosphoric acid.
[0052] M...
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