Preparation method of nano-particle reinforcement magnesium-based biocomposite material
A composite material and nanoparticle technology is applied in the field of preparation of nanoparticle reinforced magnesium-based biocomposite materials, which can solve the problems of high corrosion rate and poor plasticity of composite materials, improve comprehensive performance, refine magnesium alloy matrix grains, The effect of improving uniformity
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[0025] A method for preparing nano-particle-reinforced magnesium-based biocomposite materials uses a combination of melt shear stirring and equal-channel angular extrusion to prepare a particle-reinforced metal-based composite material. The steps are as follows:
[0026] 1) at 10 -3 Under Pa vacuum conditions and argon protection, the base alloy raw material is kept at a temperature of 720°C until it is completely melted to obtain a melt. The base alloy raw material is a magnesium alloy, and the alloying elements in the magnesium alloy are Zn and Ca. The mass of the constituent elements is: 958.89g of pure magnesium particles, 20g of zinc particles, and 11.11g of Ca particles;
[0027] 2) Pre-heat treatment of Ca-P ceramic particles with a particle size of 400-500nm at a temperature of 200°C for 2h, and then mix and grind 10g of Ca-P ceramic particles with 10g of pure magnesium particles, and the grinding time is 120min ;
[0028] 3) Add 20g of the above-mentioned ...
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