Preparation method of Metanil yellow G
An acid golden yellow, production method technology, applied in chemical instruments and methods, azo dyes, organic dyes, etc., can solve the problem of undisclosed technical data, and achieve the goal of improving output and quality, reducing production, and protecting the environment. Effect
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[0020] A kind of preparation method of embodiment acid golden yellow G, concrete preparation steps are as follows:
[0021] (1) Diazotization reaction
[0022] Add quantitative water to the diazotization reaction kettle, then add quantitative m-aminobenzenesulfonic acid, stir for 1 hour to make it a uniform suspension, add hydrochloric acid quantitatively into the reaction kettle through a metering tank, add an appropriate amount of ice to cool down to 5°C, and The sodium nitrite solid and water are added into the dissolving tank and stirred to dissolve, and the dissolved sodium nitrite solution is added into the reaction kettle, and stirred for 1 hour.
[0023] (2) Coupling reaction
[0024] Add the diazo solution prepared above into the coupling tank, add diphenylamine emulsion at 20°C, act on it to pH = 1.5, adjust pH = 4.3 with soda ash solution, keep at 13°C until the diazo compound disappears, and then Stir for 30 minutes to produce acidic golden yellow G, adjust the p...
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