A kind of offset printing ink and preparation method thereof
A technology of offset printing and ink, which is applied in the field of offset printing ink and its preparation, can solve the problems of high luminous brightness, and achieve the effects of high luminous brightness, not easy to produce defects, and strong broadband absorption capacity
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Embodiment 1
[0013] 1. Preparation of YVO 4 :Eu 3+ ,Sr 2+ Nano phosphor
[0014] (1) Add 1.2mmol Na 3 VO 4 12H 2 O was dissolved in a mixed solution containing 5ml of ethylene glycol and 2ml of distilled water; (2) While ultrasonically stirring the above solution (80kHz ultrasonic vibration and 300r / min centrifugal speed stirring), dropwise added 1.5mmol of a certain proportion of Y ( NO 3 ) 3 ·6H 2 O, Eu(NO 3 ) 3 , Sr(NO 3 ) 2 (0.9:0.03:0.07) in 8 ml of ethylene glycol solution, then ultrasonically stirred (80kHz ultrasonic vibration and 300r / min centrifugal speed stirring) for 10min until the solution was clear, and 20ml of distilled water was added; (3) Pour the reaction solution into a volume of In a 50 ml polytetrafluoroethylene-lined autoclave, under vacuum, 200 o C under heat preservation reaction 1h, down to 150 o C under insulation reaction 1h, after the end of the reaction, cooled to room temperature. The resulting suspension was poured out, centrifuged and washed ...
Embodiment 2
[0022] On the basis of embodiment 1, the YVO in the step 3 4 :Eu 3+ ,Sr 2+ with YVO 4 :Eu 3+ , Bi 3+ The weight ratio is changed to 1:0.5, and the rest are the same as in Example 1.
Embodiment 3
[0024] On the basis of embodiment 1, the YVO in the step 3 4 :Eu 3+ ,Sr 2+ with YVO 4 :Eu 3+ , Bi 3+ The weight ratio was changed to 1:0.001, and the rest were the same as in Example 1.
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