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A single barrel capillary rheometer

A capillary rheometer and capillary technology, applied in the field of high polymer rheology testing, can solve the problems of high cost, low accuracy of data results, complex structure, etc., to improve accuracy, reduce the influence of human factors, and eliminate inlet pressure. drop effect

Inactive Publication Date: 2018-09-25
TAIYUAN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Generally, there is only one capillary die in the barrel of the single-barrel capillary rheometer used in the test. Although the structure is simple, it is necessary to replace the capillary dies with different length-to-diameter ratios many times during the test to perform Bagley calibration. Obtain the rheological properties of polymer materials, because the situation of each feeding cannot be completely reproduced, the final data results are not accurate
The double-barrel capillary rheometer adopts the structure of parallel capillary die. Compared with the single-barrel capillary rheometer, it can not only improve the test efficiency, but also reduce the error caused by the experimental equipment. However, the double-barrel capillary rheometer The structure is more complicated and the cost is higher

Method used

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  • A single barrel capillary rheometer
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Embodiment Construction

[0017] In order to understand the technical solution of the present invention more clearly, the present invention will be further described below with reference to the accompanying drawings.

[0018] Such as Figure 1 to Figure 4 As shown in the figure, a single-cylinder capillary rheometer includes a cylinder 2. The front end of the cylinder 2 is provided with a plunger 1, the rear end is provided with a movable nut 6, and an electric heater 2 is arranged around the cylinder. The long capillary die 9, the supporting member 8 and the zero-length capillary die / short capillary die 7, the upper end of the plunger 1 is connected with a servo motor, and also includes a first pressure sensor 4 and a second pressure sensor 5. The first pressure sensor 4 is close to the upper end of the long capillary die, and the second pressure sensor is close to the supporting member 8. The long capillary die 9 and the zero-length capillary die / short capillary die 7 are in series, A supporting member...

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Abstract

The invention discloses a single-feed-cylinder capillary rheometer. A feed cylinder of the capillary rheometer is a single feed cylinder; the front end of the feed cylinder is provided with a plunger, the rear end of the feed cylinder is provided with a traveling nut, an electric heater is arranged around the feed cylinder, a long capillary die, a support part and a zero-length capillary die / short capillary die are arranged in the feed cylinder, and the outer diameter of the long capillary die, the outer diameter of the zero-length capillary die / short capillary die and the outer diameter of the support part all are matched with the inner diameter of the feed cylinder. The single-feed-cylinder capillary rheometer can be used for measuring extensional flow and shear flow parameters of polymer melt simultaneously, can eliminate entry pressure drop well, has the same function as a double-feed-cylinder capillary rheometer, and also has the advantages of saving raw materials, facilitating dismounting, purging easily, reducing artificial influences, realizing higher precision, and the like.

Description

Technical field [0001] The invention belongs to the technical field of high-polymerization logistic testing technology, and in particular relates to a single-barrel capillary rheometer. Background technique [0002] One of the central tasks of polymer materials research is to have a fundamental understanding and understanding of the fluidity of polymer materials. Rheometers are precisely instruments for measuring the rheological properties of polymer materials. The rheometer can simulate the actual process and production environment, determine and analyze the rheological properties of the measured polymer materials, and the data obtained can be directly used in the production and processing of polymer materials. [0003] The commonly used rheometers mainly include capillary rheometers, torque rheometers and rotational rheometers. The capillary rheometer is similar to the material flow in most processing and molding processes. It can not only measure the viscosity of the material, ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N11/04
CPCG01N11/04
Inventor 杨惠弟李振中覃富忠田生喜
Owner TAIYUAN INST OF TECH
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