Novel light-emitting compound and organic light-emitting element comprising same
A light-emitting compound and chemical formula technology, applied in the field of new light-emitting compounds and organic light-emitting elements, can solve the problems of practical difficulties, high driving voltage, low efficiency, etc., and achieve the effects of excellent element characteristics, long life, and high efficiency
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Embodiment 1
[0140] Embodiment 1: the synthesis of compound 1
[0141]
[0142] In a round bottom flask, dissolve 3.0 g of intermediate A and 3.4 g of (10-phenylanthracene-9-yl) boric acid in 100 ml of toluene, and add 15 ml of K 2 CO 3 (2M) and 0.33g of Pd(PPh 3 ) 4 , and then reflux stirring. The reaction was confirmed by TLC, and if the reaction was complete, water was added, and the organic layer was extracted with MC. After filtration under reduced pressure, it was purified on a column to obtain 2.0 g of compound 1 (yield 43%).
Embodiment 2
[0143] Embodiment 2: the synthesis of compound 2
[0144]
[0145] In a round bottom flask, dissolve 3.0 g of Intermediate A and 4.0 g of (10-(naphthalene-2-yl)anthracen-9-yl)boronic acid in 105 ml of toluene, and add 15 ml of K 2 CO 3 (2M) and 0.33g of Pd(PPh 3 ) 4 , and then reflux stirring. The reaction was confirmed by TLC, and if the reaction was complete, water was added, and the organic layer was extracted with MC. After filtration under reduced pressure, it was purified on a column to obtain 2.1 g of compound 2 (yield 40%).
Embodiment 3
[0146] Embodiment 3: the synthesis of compound 3
[0147]
[0148] In a round bottom flask, dissolve 3.0 g of Intermediate A and 4.0 g of (10-(naphthalene-1-yl)anthracen-9-yl)boronic acid in 105 ml of toluene, and add 15 ml of K 2 CO 3(2M) and 0.33g of Pd(PPh 3 ) 4 , and then reflux stirring. The reaction was confirmed by TLC, and if the reaction was complete, water was added, and the organic layer was extracted with MC. After filtration under reduced pressure, it was purified on a column to obtain 2.3 g of compound 3 (yield 44%).
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