Novel light-emitting compound and organic light-emitting element containing same
A light-emitting compound and chemical formula technology, applied in the field of new light-emitting compounds and organic light-emitting elements, can solve the problems of practical difficulties, high driving voltage, low efficiency, etc., and achieve the effects of excellent element characteristics, long life, and high efficiency
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Embodiment 1
[0140] Example 1: Synthesis of Compound 1
[0141]
[0142] In a round bottom flask, 3.0 g of Intermediate A and 3.4 g of (10-phenylanthracene-9-yl)boronic acid were dissolved in 100 ml of toluene, and 15 ml of K was added. 2 CO 3 (2M) and 0.33g of Pd(PPh 3 ) 4 , And then reflux and stir. The reaction was confirmed by TLC, and if the reaction was completed, water was added, and then the organic layer was extracted with MC. After filtration under reduced pressure, it was purified on a column to obtain 2.0 g of compound 1 (yield: 43%).
Embodiment 2
[0143] Example 2: Synthesis of Compound 2
[0144]
[0145] In a round bottom flask, 3.0g of Intermediate A and 4.0g of (10-(naphthalene-2-yl)anthracene-9-yl)boronic acid were dissolved in 105ml of toluene, and 15ml of K was added. 2 CO 3 (2M) and 0.33g of Pd(PPh 3 ) 4 , And then reflux and stir. The reaction was confirmed by TLC, and if the reaction was completed, water was added, and then the organic layer was extracted with MC. After filtration under reduced pressure, it was purified on a column to obtain 2.1 g of compound 2 (yield 40%).
Embodiment 3
[0146] Example 3: Synthesis of Compound 3
[0147]
[0148] In a round bottom flask, 3.0 g of Intermediate A and 4.0 g of (10-(naphthalene-1-yl)anthracene-9-yl) boric acid were dissolved in 105 ml of toluene, and 15 ml of K was added. 2 CO 3 (2M) and 0.33g of Pd(PPh 3 ) 4 , And then reflux and stir. The reaction was confirmed by TLC, and if the reaction was completed, water was added, and then the organic layer was extracted with MC. After filtration under reduced pressure, it was purified on a column to obtain 2.3 g of compound 3 (yield 44%).
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