A spherical lanthanum oxide
A lanthanum oxide, spherical technology, applied in rare earth metal oxides/hydroxides, inorganic chemistry, rare earth metal compounds, etc., can solve the problems of cumbersome operation methods, low catalytic efficiency of motor vehicle exhaust, etc., and achieve uniform product morphology, Reduce nucleation and growth rate, good dispersion effect
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[0029] A kind of spherical lanthanum oxide is prepared, comprising the following steps:
[0030] (1) Weigh La(NO 3 ) 3 ·6H 2 O was dissolved in the mixture of deionized water and ethylene glycol, stirred until it was completely dissolved, then added polyvinylpyrrolidone (PVP, molecular weight M=58000), stirred for about 1 hour to obtain a transparent and clear solution, added propionic acid, and continued to stir 0.5h;
[0031] (2) Transfer the transparent and clear mixed solution into a 100ml polytetrafluoroethylene lining, put it into a stainless steel reactor, and react at 200°C for 200min;
[0032] (3) After the reactor was cooled to room temperature, the product was centrifuged at a speed of 10000r / min for 5min to obtain a precipitate, which was washed alternately with deionized water and ethanol for 3 times, and then dried at 80°C for 12h to obtain lanthanum oxide.
[0033] Test preparation: (1) Dry the lanthanum oxide prepared in Example 1, and grind it into a fine ...
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