Preparation technology of tea saponin-containing liquid shampoo

A technology for tea saponin and shampoo, which is applied to the extraction of tea saponin by microwave-assisted enzymatic method and its application in shampoo, can solve the problems of low product purity, low extraction efficiency, long time consumption, etc., and achieves improvement of hair follicle absorption. , hair soft, easy-to-manage effect

Inactive Publication Date: 2017-05-31
张仕英
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The current methods for extracting tea saponin from tea seed meal mainly include water extraction, water extraction-precipitation, organic solvent extraction, etc., but these methods generally have disadvantages such as low extraction efficiency, long time-consuming, and low product purity.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A kind of preparation technology of the shampoo containing tea saponin, it is characterized in that comprising the following steps:

[0019] (1) Extraction of tea saponin

[0020] Grind the deoiled tea seed meal to obtain a powder with a particle size of 20 mesh, prepare a suspension with water at a mass ratio of 1:20, and treat it with microwaves for 10 minutes at 70°C with a processing power of 300W. After treatment, cool the suspension to 40°C, adjust the pH to 4.5, add 1% cellulase, microwave-assisted enzymolysis for 40min, microwave power 350W, inactivate the enzyme in a water bath at 100°C for 10min, centrifuge at 5000r / min for 30min, and collect the supernatant Obtain tea saponin. The frequency of the microwave processor used is 915 MHz or 2450 MHz;

[0021] (2) Formulation preparation

[0022] Calculate the shampoo formula (by mass percentage) of tea saponin in a certain proportion as follows:

[0023] Coconut Diethanolamide 3%;

[0024] Cocopropyl Betaine ...

Embodiment 2

[0034] A kind of preparation technology of the shampoo containing tea saponin, it is characterized in that comprising the following steps:

[0035] (1) Extraction of tea saponin

[0036] Crush the deoiled tea seed meal to obtain a powder with a particle size of 25 meshes, prepare a suspension with water at a mass ratio of 1:20, and treat it with microwaves for 12.5 minutes at 80°C with a processing power of 275W, and cool the suspension after treatment To 45°C, adjust the pH to 5.5, add 2% cellulase, microwave-assisted enzymolysis for 35min, microwave power 375W, inactivate the enzyme in a water bath at 100°C for 15min, centrifuge at 7500r / min for 25min, collect the supernatant Tea saponins are available. The frequency of the microwave processor used is 915 MHz or 2450 MHz;

[0037] (2) Formulation preparation

[0038] Calculate the shampoo formula (by mass percentage) of tea saponin in a certain proportion as follows:

[0039] Coconut Diethanolamide 4%;

[0040] Cocoprop...

Embodiment 3

[0050] A kind of preparation technology of the shampoo containing tea saponin, it is characterized in that comprising the following steps:

[0051] (1) Extraction of tea saponin

[0052] Grind the deoiled tea seed meal to obtain a powder with a particle size of 30 mesh, prepare a suspension with water at a mass ratio of 1:20, and treat it with microwaves at 90°C for 15 minutes with a processing power of 250W. After treatment, cool the suspension to 50°C, adjust the pH to 6.5, add 3% cellulase, microwave-assisted enzymolysis for 30min, microwave power 400W, inactivate the enzyme in a water bath at 100°C for 20min, centrifuge at 10000r / min for 20min, and collect the supernatant Obtain tea saponin. The frequency of the microwave processor used is 915 MHz or 2450 MHz;

[0053] (2) Formulation preparation

[0054] Calculate the shampoo formula (by mass percentage) of tea saponin in a certain proportion as follows:

[0055] Coconut Diethanolamide 5%;

[0056] Cocopropyl Betaine...

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Abstract

The invention discloses a preparation technology of a tea saponin-containing liquid shampoo. The preparation technology is characterized by comprising the following steps: (1) crushing deoiled tea seed meal, preparing a suspension from water, carrying out microwave treatment at 70-90 DEG C, cooling the suspension to 40-50 DEG C after treatment, adjusting the pH to 4.5-6.5, adding 1-3% of cellulose, carrying out microwave assisted digestion for 30-40min, carrying out enzyme deactivation, centrifuging in a mixed liquid condition and collecting a supernate to obtain tea saponin; (2) calculating the dosage of various components at a certain ratio and weighing the components; and (3) adding deionized water to a mixing kettle, adding the tea saponin under the stirring condition, heating to 70-80 DEG C, stirring evenly, adding cocomut oil diethanolamide, coco amido propyl betaine and guar gum in sequence, stirring until completely dissolving, cooling to 45-50 DEG C, adding a camellia japonica extract and lavender essential oil in sequence, mixing evenly, adjusting the pH value to be 5.5-6.5 by using citric acid, stirring evenly and then cooling to obtain the tea saponin-containing liquid shampoo.

Description

technical field [0001] The invention relates to the extraction and preparation technology of tea saponin, in particular to the extraction and preparation technology of tea saponin by microwave-assisted enzymatic method, and further relates to the extraction and preparation technology of tea saponin by microwave-assisted enzymatic method and its application in shampoo. Background technique [0002] Shampoo is a hair cleaning product widely used by everyone. However, most of the strong decontamination shampoos on the market use synthetic surfactants, which are easy to damage the hair quality, while natural shampoos have insufficient decontamination ability. [0003] Tea saponin is a kind of oleanane-type pentacyclic triterpene saponin mixture extracted from tea seed dregs. It is a non-ionic surfactant with good softening, dispersing, wetting and decontamination functions. Send double function. The current methods for extracting tea saponin from tea seed meal mainly include w...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K8/9789A61K8/60A61K8/42A61K8/44A61K8/73A61K8/92A61K8/365A61Q5/02A61Q5/00A61Q5/12
CPCA61K8/602A61K8/365A61K8/42A61K8/44A61K8/737A61K8/922A61K8/97A61K2800/81A61Q5/006A61Q5/008A61Q5/02A61Q5/12
Inventor 张仕英
Owner 张仕英
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