Preparation method of hollow BiVO4 micron sheet photocatalyst
A technology of photocatalyst and micron sheet, which is applied in the direction of catalyst activation/preparation, physical/chemical process catalyst, metal/metal oxide/metal hydroxide catalyst, etc. It can solve the problems of high cost, complicated operation and difficulty in large-scale preparation , to achieve the effect of simple route, easy large-scale production and good repeatability
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[0038] The present invention will be further described below in conjunction with the accompanying drawings. It should be noted that this embodiment is based on the technical solution, and provides detailed implementation and specific operation process, but the protection scope of the present invention is not limited to the present invention. Example.
[0039] Hollow BiVO co-modified with borate ion doping and cobalt oxide nanoparticles 4 The preparation method of micron sheet photocatalyst comprises the following steps:
[0040] S1 synthesis of hollow BiVO 4 Microflakes:
[0041] 1.1) After diluting 2mL of concentrated nitric acid into 10mL of distilled water, add 5mmol of BiVO 4 ·5H 2 O, stir to make it dissolve, obtain solution A;
[0042] 1.2) Add 5mmol of NaVO 3 Add 1g of ethylenediaminetetraacetic acid into 8mL NaOH solution with a concentration of 4mmol / L, stir to dissolve, and obtain solution B;
[0043] 1.3) Add solution B to solution A, adjust the final pH of t...
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