High-sensitivity stretchable flexible strain sensor and preparation method thereof
A strain sensor, flexible technology, applied in the direction of electric/magnetic solid deformation measurement, electromagnetic measurement device, etc., can solve the problems of low stretchability, low sensitivity, poor stability, etc., achieve simple preparation method, improve Sensing performance, cost reduction effects
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[0071] Example 1
[0072] This embodiment provides a flexible strain sensor and a preparation method thereof. The method includes the following steps:
[0073] (1)' The polyurethane sponge (thickness 0.8mm, length 20mm, width 10mm) is repeatedly washed with deionized water and absolute ethanol, and then dried;
[0074] (1) Soak the dried polyurethane sponge in a graphene solution for 4 hours, and then use hot hydroiodic acid to reduce the polyurethane sponge impregnated with graphene oxide at 85°C in a water bath for 12 minutes, hydroiodic acid The concentration is calibrated as follows: make the volume ratio of deionized water in the solution of hydroiodic acid and graphene oxide 1:1, dry, and then repeat the above-mentioned soaking, reduction and drying steps 4 times, and repeat the last time After time reduction, it is washed with deionized water and then dried to obtain graphene-coated polyurethane sponge;
[0075] (2) Use the graphene-coated polyurethane sponge described in step...
Example Embodiment
[0080] Example 2
[0081] (1)' The polyurethane sponge (thickness 1mm, length 25mm, width 10mm) is repeatedly washed with deionized water and absolute ethanol, and then dried;
[0082] (1) Soak the dried polyurethane sponge in a graphene solution for 3 hours, and then use hot hydroiodic acid to reduce the polyurethane sponge impregnated with graphene oxide at 90°C in a water bath for 10 minutes, hydroiodic acid The concentration is calibrated as follows: make the volume ratio of deionized water in the solution of hydroiodic acid and graphene oxide 1:2, dry, and then repeat the above-mentioned soaking, reduction and drying steps 3 times, and repeat the last time After time reduction, it is washed with deionized water and then dried to obtain graphene-coated polyurethane sponge;
[0083] (2) Use the graphene-coated polyurethane sponge described in step (1) as the cathode, nickel foil as the anode, and NiCl 2 ·6H 2 O, H 3 BO 3 And ethylenediamine dihydrochloride mixed solution (NiCl 2 ...
Example Embodiment
[0086] Example 3
[0087] (1)' The polyurethane sponge (thickness 1.5mm, length 30mm, width 15mm) is repeatedly washed with deionized water and absolute ethanol, and then dried;
[0088] (1) Soak the dried polyurethane sponge in a graphene solution for 5 hours, and then use hot hydroiodic acid to reduce the polyurethane sponge impregnated with graphene oxide at 85°C in a water bath for 10 minutes. The concentration is calibrated as follows: make the volume ratio of deionized water in the solution of hydroiodic acid and graphene oxide 1:5, dry, and then repeat the above-mentioned soaking, reduction and drying steps twice, and repeat the last time After time reduction, it is washed with deionized water and then dried to obtain graphene-coated polyurethane sponge;
[0089] (2) Use the graphene-coated polyurethane sponge described in step (1) as the cathode, nickel foil as the anode, and NiCl 2 ·6H 2 O, H 3 BO 3 And ethylenediamine dihydrochloride mixed solution (NiCl 2 ·6H 2 O concentr...
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