Spherical powder material for 3D printing and preparation method thereof
A spherical powder, 3D printing technology, applied in the field of 3D printing, can solve the problems that the fluidity is difficult to meet the requirements, the resin powder is easy to bond, and the sphericity of the 3D printing powder is not low, and it is easy to mass production, easy to emulsify, The effect of improving the finish
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[0034] The present invention also provides a method for preparing a spherical powder material for 3D printing, comprising the following steps:
[0035] S1, the raw materials are mixed in the reactor, and then pulverized;
[0036] S2, heating up to 10°C-100°C above the melting point of the thermoplastic resin;
[0037] S3, cooling, separating, and drying to obtain a spherical powder product.
[0038] The preparation method of the spherical powder material for 3D printing in the present invention combines the advantages of the crushing method and the emulsification method. First, it is crushed in a solvent, which can reduce the temperature rise of the crushing and avoid the agglomeration of the bonded crushing tool and thermoplastic resin powder. , The thermoplastic resin powder is dispersed and emulsified in a modified silicone oil solvent (or a mixed solvent with low boiling point silicone oil), and after cooling, it can form a spherical structure and improve fluidity.
[0039...
Embodiment 1
[0047] Take 100 kg of low-density polyethylene (HDPE) resin, 250 kg of cyanosilicone oil, 100 kg of kerosene, and 2 kg of emulsifier into the emulsification kettle, heat it to about 100 degrees, start the emulsifier to shear and pulverize for 1.5 hours, and put it under the protection of nitrogen Gradually raise the temperature to about 160 degrees to emulsify for 4 hours, cool, separate with a bag centrifuge, wash with water, dry, sort and compound, and pack for shipment.
Embodiment 2
[0049] Take 100 kg of polypropylene resin, 250 kg of water-based silicone oil, 100 kg of methyl oil, and 2 kg of emulsifier into the emulsification kettle, heat to about 100 degrees, start the emulsifier to shear and pulverize for 4 hours, and gradually heat up to Emulsify at about 200 degrees for 5 hours, cool, continue solid-liquid separation, wash with water, dry, sort and compound, pack and ship.
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