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Test device for in situ study of heavy metal dynamic adsorption reaction in water

A dynamic adsorption and testing device technology, applied in the field of water treatment, can solve the problems of affecting the efficient removal of heavy metal adsorption materials in water, unable to study and analyze heavy metals adsorption by materials, and difficult to effectively explore the heavy metal adsorption mechanism.

Active Publication Date: 2018-11-23
ANHUI UNIVERSITY OF ARCHITECTURE
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] In order to solve the problem in the background technology that there is currently no device capable of using in-situ QXAFS technology for real-time analysis and research on the dynamic process of heavy metal adsorption by materials in a solution system, it is impossible to realize real-time research and analysis on the dynamic process of heavy metal adsorption by materials, and then It is difficult to effectively explore the adsorption mechanism of heavy metals in the initial process of adsorption, which will eventually affect the research and development of adsorption materials for the efficient removal of heavy metals in water. To provide a test device for in situ research on the dynamic adsorption reaction of heavy metals in water, it can use in situ synchrotron radiation Study on dynamic adsorption process of heavy metals in solution by QXAFS method

Method used

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  • Test device for in situ study of heavy metal dynamic adsorption reaction in water
  • Test device for in situ study of heavy metal dynamic adsorption reaction in water
  • Test device for in situ study of heavy metal dynamic adsorption reaction in water

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Embodiment 1

[0024] like Figure 1-Figure 3 Shown, a kind of testing device of in situ researching the dynamic adsorption reaction of heavy metals in water, said device comprises reactor 1, offers on reactor 1 the incident window 16 that can communicate with external environment and reactor interior, described incident window The surface where 16 is located serves as the front of the reactor 1, and the back of the reactor is provided with an exit window corresponding to the position of the entrance window, and a sealing film is provided on the entrance window and the exit window; the bottom of the reactor is provided with a multi-dimensional adjustment platform 15 for multi-dimensional adjustment The platform can translate along the three directions of X, Y, and Z, and can rotate in the horizontal direction; the top of the reactor is provided with a feed port 2, and the inside of the reactor is provided with a reversible electromagnetic plate 3 corresponding to the position of the feed port...

Embodiment 2

[0039] Such as Figure 1-Figure 3 Shown, a kind of testing device of in situ researching the dynamic adsorption reaction of heavy metals in water, said device comprises reactor 1, offers on reactor 1 the incident window 16 that can communicate with external environment and reactor interior, described incident window The surface where 16 is located serves as the front of the reactor 1, and the back of the reactor is provided with an exit window corresponding to the position of the entrance window, and a sealing film is provided on the entrance window and the exit window; the bottom of the reactor is provided with a multi-dimensional adjustment platform 15 for multi-dimensional adjustment The platform can translate along the three directions of X, Y, and Z, and can rotate in the horizontal direction; the top of the reactor is provided with a feed port 2, and the inside of the reactor is provided with a reversible electromagnetic plate 3 corresponding to the position of the feed p...

Embodiment 3

[0055] A test device for in-situ research on the dynamic adsorption reaction of heavy metals in water. The application of the in-situ research on the dynamic process of heavy metal adsorption in water is as follows:

[0056]1. Fix the reaction device to the position where solid samples are commonly used in the synchrotron radiation QXAFS experimental station, and place an X-ray fluorescent plate consistent with the size of the window at the incident and exit windows 16 of the reserved polyimide film, from X, Y Rotate and adjust the adjustment platform 15 at the bottom in the three directions of X, Z and in the horizontal plane, so that the incident and outgoing X-rays are facing the center of the exit window 16, and record the X, Y, Z three directions of the adjustment platform and the angles in the horizontal plane. parameter, keep the position unchanged, and remove the X-ray fluorescent plate used for calibration;

[0057] 2. Place a magnetic stirrer from the feed port 2 of ...

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Abstract

The invention discloses a test device for in situ study of heavy metal dynamic adsorption reaction in water. The test device comprises a reactor, wherein an incidence window used for communicating outside environment with the inside of the reactor is formed in the reactor; the located surface of the incidence window is used as the front side of the reactor; an emergence window is arranged in the position, corresponding to the incidence window, at the back side of the reactor; a sealing film is arranged on the incidence window and the emergence window; a multidimensional regulation platform isarranged at the bottom of the reactor and can transversely move in the three directions X, Y and Z and can rotate in the horizontal direction; a feeding opening is formed in the top of the reactor; anelectromagnetic flat plate capable of turning and rotating is arranged inside the reactor. The device also comprises a capillary tube focusing lens; the capillary tube focusing lens is positioned atone side of the front side of the reactor. By using the device, the process of studying the dynamic adsorption process of the material on heavy metals in the solution by an in situ synchronous radiation QXAFS method can be achieved; the yield, the quality, the precision and the efficiency are improved.

Description

technical field [0001] The invention relates to the technical field of water treatment, in particular to a test device for in-situ research on the dynamic adsorption reaction of heavy metals in water. Background technique [0002] Drinking water safety is one of the most challenging issues facing mankind at present. Many areas are currently facing the problem of excessive heavy metals in drinking water. The methods and materials for removing heavy metals in water are currently a research topic of widespread concern at home and abroad. At present, there are many methods for removing heavy metals in water, such as coagulation method, adsorption method, ion exchange method, membrane method and so on. Among them, the adsorption method is a relatively common method used in water treatment processes in recent years. It has the characteristics of simple device, easy to use, and stable operation effect. At the same time, the use of adsorption-desorption can achieve the effect of reg...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N23/085
CPCG01N23/085
Inventor 孙柏丁晨风王辉范萍邓阳红鲁永鹏张靖敏王磊
Owner ANHUI UNIVERSITY OF ARCHITECTURE
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