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Fingerprint spectrum establishing method for controlling processing process parameters of wine-soaked cornus officinalis Sieb.et Zucc.

A technology of fingerprint and establishment method, which is applied in the field of establishment of fingerprints for controlling the processing parameters of Cornus officinalis, can solve the problems of uncertainty of specific parameters, no clear research, no better research, etc.

Inactive Publication Date: 2019-07-05
JIUZHITANG
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although Cornus officinalis is steamed with wine according to the general rule 0213 of the Pharmacopoeia, the specific parameters are not sure. Glycosides) and toxic components (5-hydroxymethylfurfural) have an impact, so far there is no clear research
[0005] At present, through the establishment of the fingerprints of Cornus officinalis, the processing technology and parameters of the five index components before and after processing are used to optimize the processing technology and parameters, so as to effectively control the active and controlling components (5-hydroxymethyl) in the processing of Cornus officinalis. There is no good research in the field of furfural

Method used

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  • Fingerprint spectrum establishing method for controlling processing process parameters of wine-soaked cornus officinalis Sieb.et Zucc.
  • Fingerprint spectrum establishing method for controlling processing process parameters of wine-soaked cornus officinalis Sieb.et Zucc.
  • Fingerprint spectrum establishing method for controlling processing process parameters of wine-soaked cornus officinalis Sieb.et Zucc.

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] 1. Reagents and reagents

[0041] Gallic acid (batch number: 110831-200302, for content determination, China Institute for the Control of Pharmaceutical and Biological Products); protocatechuic acid (batch number: 110809-200604, for content determination, China Institute of Pharmaceutical and Biological Products); 0424121, Tianjin Yifang Biotechnology Co., Ltd.); loganin (batch number: 11640-200502, for content determination, China National Institute of Pharmaceutical and Biological Products); 5-Hydroxymethylfurfural (batch number: 070102, for content determination, Shanghai Yousi Biotechnology Co., Ltd.); Cornus officinalis (produced in Henan, Jiuzhitang Co., Ltd., FM161005); acetonitrile was chromatographically pure (US TEDIA Company), water was ultrapure water, methanol (Sinopharm Group, AR).

[0042] 2. Instrument

[0043] Shimadzu LC-20A; LCSolution (Shimadzu Corporation of Japan); ZORBAX SB C-18 analytical column (4.6mm × 250mm, 5μm, American Agilent Company); KQ...

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Abstract

The invention discloses a fingerprint spectrum establishing method for controlling the processing process parameters of wine-soaked cornus officinalis Sieb.et Zucc. According to the method, the processing process parameters, namely, the content (peak area) of loganin, morroniside, gallic aci, protocatechuic acid, and 5-hydroxymethyl furfural, in a fingerprint spectrum in a processing process are controlled, so that the processing technology of the wine-soaked cornus officinalis Sieb.et Zucc. can be controlled. The influence of each of the three factors of processing time, covered moistening time and steaming time on the five chemical components before and after the processing is investigated, so that optimal processing time, covered moistening time and steaming time can be confirmed.

Description

technical field [0001] The invention relates to the technical field of traditional Chinese medicine processing, in particular to a fingerprint establishment method for controlling processing parameters of dogwood officinalis. Background technique [0002] Cornus officinalis is the dried and mature pulp of Cornus officinalis Sieb.et Zucc., a plant of the family Cornaceae; it was first recorded in "Shen Nong's Herbal Classic". It is sour, astringent, slightly warm, and returns to the liver and kidney channels; it has the effects of nourishing the liver and kidney, astringent and astringent. The medical sage Zhang Zhongjing formulated the "Jingui Shenqi Pill" with Cornus officinalis as the king's medicine; the Song Dynasty imperial physician Qian Yi's "Children's Medicine Syndrome Zhijue" deleted the Shenqi Pill and the prescription "Dihuang Pill" also contained " Cornus officinalis" is used to nourish kidney yin and treat children's bedwetting and other diseases. Later, it i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/02G01N30/06
CPCG01N30/02G01N30/06G01N2030/027
Inventor 邓芸黄胜叶惠煊周良袁莉袁利群
Owner JIUZHITANG
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