Full-automatic urine iodine and water iodine analyzer and analysis method
An analyzer, fully automatic technology, applied in the direction of color/spectral characteristic measurement, test sample preparation, etc., can solve the problem that the sample cannot be fully automatic digestion, etc., achieve fast automatic detection, meet fast analysis, and high work efficiency Effect
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Embodiment 1
[0044] This embodiment provides a fully automatic urine iodine and water iodine analyzer, which can realize the automatic addition of reagents, automatic stirring and automatic detection, and can realize automatic digestion of samples, automatic heat preservation and automatic detection; the fully automatic urine iodine And water iodine analyzer comprises analyzer body, and this analyzer body comprises workbench and the three-dimensional movement platform that is arranged on described workbench, graphite digestion device, water bath container, sample holder, vortex mixing shaker, cleaning device and detection device.
[0045] Wherein, the three-dimensional motion platform can realize three-dimensional translation of the X-axis, Y-axis and Z-axis, and a manipulator is installed on the Z-axis of the three-dimensional motion platform, and the manipulator is used to grab the sample tube.
[0046] In this embodiment, three sampling capillaries are provided on the manipulator, so as...
Embodiment 2
[0062] The present embodiment provides a kind of analytical method of urinary iodine, and it utilizes the automatic urine iodine described in embodiment 1 and water iodine analyzer to realize, and comprises:
[0063] S10. Add an appropriate amount of distilled water, such as 20L, into the hot water circulation device and the water bath container, and make the hot water circulation device add or extract an appropriate amount of water, such as 1L, into the water bath container 2 through the circulation pipeline. The temperature of the water in the water bath container 2 and the hot water circulation device is the same, and in this embodiment, the temperature is set to 30°C.
[0064] S15, take out the first sample rack 3a and the second sample rack 3b, put the sample tubes containing 0.25ml urine sample on the sample rack in turn; then put the sample rack into the water bath container 2;
[0065] S20, sequentially add 1 mL of ammonium persulfate solution to the sample tube of the...
Embodiment 3
[0076] The present embodiment provides a kind of analysis method of water iodine, and it utilizes the full-automatic urine iodine described in embodiment 1 and water iodine analyzer to realize, and comprises:
[0077] S10. Add an appropriate amount of distilled water, such as 20L, into the hot water circulation device and the water bath container, and make the hot water circulation device add or extract an appropriate amount of water, such as 1L, into the water bath container 2 through the circulation pipeline. The temperature of the water in the water bath container 2 and the hot water circulation device is the same, and in this embodiment, the temperature is set to 30°C.
[0078] S15, take out the first sample rack 3a and the second sample rack 3b, put the sample tubes with 10ml water sample on the sample rack in turn; then put the sample rack into the water bath container 2;
[0079] S20. Add 1mL of sodium chloride solution, 0.5mL of arsenous acid solution, and 1.0mL of sul...
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