Patents
Literature
Patsnap Copilot is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Patsnap Copilot

34results about How to "Meet the needs of rapid analysis" patented technology

A method for rapid and non-destructive analysis of nutritional quality of whole cottonseed based on near-infrared spectroscopy

The invention provides a novel fast and non-destructive analysis method for the nutritional quality of cottonseed. The method comprises the following steps: 1) selecting whole cottonseeds of representative cotton varieties as experimental samples; 2) using a near-infrared spectrometer to collect near-infrared spectral data of whole cottonseeds, and the spectral scanning range is 800-2500nm; 3) using the national standard method Accurately analyze the nutritional quality of cottonseed; 4) Preprocess the near-infrared spectrum data; 5) Select spectral variables to eliminate non-informative variables; 6) Use the multivariate correction method to establish the near-infrared spectrum of whole cottonseed and the nutritional value of whole cottonseed 7) Performance evaluation of the calibration model; 8) Collect near-infrared spectral data of the whole cottonseed to be tested, and use the calibration model to predict its nutritional quality after preprocessing the spectral data. The invention has fast analysis speed, does not destroy samples, does not require sample pretreatment, has high detection accuracy, and can analyze various nutritional quality components in cotton seeds at the same time, and provides a convenient, fast and efficient analysis method for cotton breeding and cotton seed inspection.
Owner:ZHEJIANG UNIV

Low field nuclear magnetic resonance-applied frozen beef freshness nondestructive testing method

The invention discloses a low field nuclear magnetic resonance-applied frozen beef freshness nondestructive testing method. The low field nuclear magnetic resonance-applied frozen beef freshness nondestructive testing method comprises the following steps of (A) sample collection, (B) sample measurement, (C) sample low field nuclear magnetic analysis, (D) multiple freshness-related index measurement, (E) model establishment, (F) model assessment and (G) measurement of freshness of samples to be detected. By establishing a mathematical predication model reflecting fresh beef moisture content relaxation spectrum information and multiple indexes related to fresh beef freshness to accurately and reliably detect multiple indexes of an unknown fresh beef simultaneously such as thiobarbituric acidreactive substances (TBARS), volatile basic nitrogen (TVB-N) and pH, the low field nuclear magnetic resonance-applied frozen beef freshness nondestructive testing method can help predict the storagetime of the beef and achieve rapid and nondestructive detection and assessment of the freshness of the fresh beef. The low field nuclear magnetic resonance-applied frozen beef freshness nondestructivetesting method is rapid and accurate, avoids influence of beef surface properties, and during measurement, has no damage to the beef.
Owner:DALIAN POLYTECHNIC UNIVERSITY

Method for quickly separating copper matrix for ICP-MS analysis of impurity elements in metal copper

The invention relates to a method for quickly separating a copper matrix for ICP-MS analysis of impurity elements in metal copper, which comprises the following steps: digesting a metal copper sampleby using a mixed acid solution of nitric acid and sulfuric acid (a small amount) in a certain ratio, and removing the copper matrix by using a high-current quick electrolysis method to obtain a solution to be detected; and then adopting inductively coupled plasma mass spectrometry (ICP-MS) to realize rapid and simultaneous determination of twelve impurity elements of arsenic, antimony, tellurium,tin, lead, zinc, iron, nickel, cobalt, chromium, cadmium and manganese in the to-be-detected solution under certain instrument working conditions. Compared with the national standard GB / T 5121.28-2010, the method has the advantages that the separation effect is good, the matrix interference is eliminated, the twelve impurity elements of arsenic, antimony, tellurium, tin, lead, zinc, iron, nickel,cobalt, chromium, cadmium and manganese can be rapidly and simultaneously determined, the measurement time is short, and the requirement of rapid analysis of the twelve trace impurity elements in themetal copper is met.
Owner:北矿检测技术股份有限公司

Semi-quantitative detection method of quaternary ammonium salt of water quality

The invention discloses a semi-quantitative detection method of quaternary ammonium salt of water quality. The method comprises the following steps: sucking a water sample to be detected into a reaction tube, dripping a quaternary ammonium salt detection reagent into the reaction tube, uniformly shaking, then immediately carrying out color comparison between the color of the shaken solution and a testing standard color card, and determining the content of the quaternary ammonium salt by comparing the color of the shaken solution with the testing standard color card, wherein the quaternary ammonium salt detection reagent comprises titan yellow, ethylene diamine tetraacetic acid (EDTA), Thymol blue and sodium hydroxide, and is prepared by mixing the titan yellow, the EDTA, the Thymol blue and the sodium hydroxide according to the mass ratio of 100: (5-100): (20-200): (10-100). According to the method, the concentration of the quaternary ammonium salt in the water sample can be rapidly detected only by the quaternary ammonium salt detection reagent, the reaction tube and the testing standard color card; the method is simple to operate, can be operated in real time on site, and meets the demand of rapidly analyzing a great deal of samples.
Owner:ZHEJIANG UNIV

Device and method for analyzing Sr-90 in reactor decommissioned stainless steel material

The invention discloses a device and method for analyzing Sr-90 in a reactor decommissioned stainless steel material. The device is divided into a separating unit and a measuring unit; the separatingunit achieves rapid separation of the Sr-90 and a daughter Y-90 of the Sr-90; the measuring unit measures the activity concentration of the separated and purified daughter Y-90 of the Sr-90; and thenthe activity concentration of the Sr-90 is calculated according to the Y-90. According to the method, the treating time is short, and the requirements of rapid separation and analysis are met; meanwhile, the analysis process is simplified and controllable, the using amount of chemical reagents and the contact time of workers are reduced, and the adverse effects of hazards of radioactive reagents and the chemical reagents on occupational health of the workers are avoided; and moreover, according to the principle of selective adsorption separation, the daughter Y-90 of the Sr-90 is efficiently adsorbed and desorbed, and the high recovery efficiency is guaranteed. The method has the advantages of short separation time, simple process, high recovery rate, good system stability, long service life and the like, and the needs of rapid analysis of the Sr-90 in the stainless steel material in a reactor can be met.
Owner:INST OF NUCLEAR PHYSICS & CHEM CHINA ACADEMY OF

Method for quickly determining content of barium in nickel salt solution

InactiveCN109142246ALarge amount allowedCo-precipitation has little effectColor/spectral properties measurementsMicrogramNickel salt
The invention discloses a method for quickly determining the content of barium in a nickel salt solution. In 0.12 mol/L of hydrochloric acid medium, tribromoarsenazo and barium can form a stable purple complex, and according to the spectrophotometric analysis principle, accurate determination of the content of the barium in a nickel chloride solution or a nickel nitrate solution is completed. Themethod comprises the specific steps that 5.0 mL of 0.6 mol/L hydrochloric acid solution and 2.0 mL of 50 g/L ascorbic acid solution are added into the pretreated nickel chloride or nickel nitrate solution in a 25 mL volumetric flask in sequence and mixed evenly, then 5.0 mL of 1g/L tribromoarsenazo solution is added, and the volume is metered; with the reagent blank as a reference, the absorbancyis measured at the wave length of 620 nm, and according to the absorbancy value, the content of the barium in the to-be-measured solution is obtained on a working curve. By means of the method, the content of the barium is within the range from 0 microgram/25 mL to 50 micrograms/25 mL and accords with the Beer's law, and the apparent molar absorption coefficient epsilon is 4.64*10<4>Lmol<-1>cm<-1>; the recycling rate is 95-103%, RSD is smaller than 10%, the method is stable, reliable, quick and simple, and requirements for quick analysis of the barium in the nickel chloride and nickel nitrateproduction process can be met.
Owner:JINCHUAN GROUP LIMITED +1

Portable disposable surface-enhanced Raman/colorimetric dual sensor as well as preparation method, detection method and application thereof

The invention relates to a portable disposable surface-enhanced Raman/colorimetric dual sensor as well as a preparation method, a detection method and application thereof. The sensor comprises a sample measuring tube and a sampling part. The sample measuring tube comprises a tube body, an opening end and a sealing end arranged at two ends of the tube body, a detection solution section arranged inthe tube body, and a closed section. The preparation method comprises the following steps: preparing an ion nanoparticle colloidal solution by adopting a sodium citrate reduction method, and injectingthe ion nanoparticle colloidal solution into the tube body in a vacuum state to obtain the sensor. The detection method comprises the following steps: wiping the surface of a to-be-detected object through a sampling part; breaking the closed section of the tube body to immerse a detection solution into the sampling part; and then performing colorimetric detection or in-situ SERS detection on a discoloration sampling part to obtain qualitative and quantitative analysis results. Compared with the prior art, the portable disposable surface-enhanced Raman/colorimetric dual sensor can meet the requirement for large-batch rapid analysis in a laboratory, is convenient to use at a time in pollution field detection to avoids cross contamination; and a novel portable device for fruit and vegetablepesticide residue detection, emergency analysis and judicial expertise can be provided.
Owner:SHANGHAI INSTITUTE OF TECHNOLOGY

Analytic pretreatment machine for metal material and treatment method for analytic pretreatment machine

The invention relates to an analytic pretreatment machine for a metal material, also relates to a corresponding treatment method and belongs to the technical field of metallurgy detecting and grinding equipment. The analytic pretreatment machine comprises a vertical cylindrical vacuum chamber provided with an air exhaust interface and a sealing door; the middle of the bottom surface of the vacuumchamber upwards extends to form a cathode tube connected with a high-voltage power supply; a cathode head with a placing area for a to-be-treated sample is arranged on the top of the cathode tube; a shielding device for covering the cathode head and the cathode tube is extended from the periphery of the placing area; a cooling channel which is externally connected with a cooling fluid source is arranged inside the cathode head; a grounded anode base is arranged at the middle of the top end of the vacuum chamber; the grounded anode base downwards extends to form an anode head opposite to the cathode head; an inert gas feeding pipe is arranged in the anode head; and a gas exhausting port of the gas feeding pipe is opposite to the sample placing area of the cathode head. Due to the adoption of the analytic pretreatment machine and the treatment method disclosed by the invention, secondary oxidation can be avoided; excellent effect and high speed can be obtained; and the demand for quick analysis can be better met, and thereby a more accurate detection result is obtained.
Owner:NANJING HEAO ELECTROMECHANICAL EQUIP

Rapid determination of total iron content in vanadium titanomagnetite

The rapid determination method of total iron content in a kind of vanadium-titanium magnetite provided by the invention comprises: 1) taking by weighing the vanadium-titanium magnetite sample whose weight is M; 2) adding a sufficient amount of ore dissolving solution to be measured Vanadium-titanium-magnetite sample is heated and dissolved; 3) Add dilute hydrochloric acid in the reaction vessel; 4) Then dropwise add tin protochloride solution to light yellow, heat to slightly boiling again, then cool to room temperature; 5) Add to the reaction vessel Add sodium tungstate solution to the container, drop titanium trichloride solution to blue, and add dropwise titanium trichloride solution to a slight excess; 6) then drop potassium dichromate solution to colorless, and add diphenylamine sulfonate dropwise sodium acid indicator; 7) titrate to purple with potassium dichromate standard titration solution; 8) measure the weight percentage of vanadium in the solution after titration to purple; 9) calculate the steps. The method is simple in operation, fast in determination speed, and the test results are comparable to the national standard method, which can better meet the needs of on-site rapid analysis.
Owner:武汉钢铁有限公司

A rapid and non-destructive detection method for moisture content in abalone drying and rehydration process

The invention relates to a method for rapid and nondestructive detection of the water content in the abalone drying and rewatering process. The method comprises the following steps: acquiring echo attenuation curve data of fresh abalone samples, drying the fresh abalone samples, and acquiring the CPMG signals of the fresh abalone samples in the drying process; rewatering the dried abalone samples after the echo attenuation curve data of the fresh abalone samples is acquired, and acquiring the CPMG signals of the dried abalone samples in the rewatering process; determining the real water content of every sample; establishing a water content predicating model corresponding to the real water content in the drying and rewatering process; and acquiring the echo attenuation curve data of an abalone sample to be detected through adopting the same technology, and combining with the water content predicating model to obtain the predicated value of the water content of the abalone sample to be detected. The method has the advantages of high measurement result accuracy, short time, no damages to abalones, fastness, and no pretreatment of the abalones, and can realize rapid and nondestructive detection of the water content of the abalone drying and rewatering process.
Owner:DALIAN POLYTECHNIC UNIVERSITY

An Analytical Method for Limiting Short-Circuit Current Using Line Out-of-Series Operation

The invention relates to an analytical method of limiting short-circuit current by utilizing circuit serial operation. The analytical method of limiting the short-circuit current by utilizing circuit serial operation comprises the following steps: (1) an impedance matrix and node short-circuit current of a power grid in a initialization operation mode are calculated; (2) an equivalent circuit corresponding to the circuit serial operation is constructed, and node impedance variable quantities in different circuit serial operations are rapidly calculated; and (3) a serial operation mode when impedance variation is the largest is selected, and the corresponding short-circuit current is calculated. The technical scheme of the analytical method of limiting short-circuit current by utilizing circuit serial operation is applied to analytical calculation of the short-circuit current in an electrical power system and rapid analysis and decision of a limiting scheme of the short-circuit current. The different circuit serial operation modes in the actual operation of the power grid are different in limiting effects on the short-circuit current, the short-circuit current is effectively limited by selecting an appropriate circuit serial operation mode, assistance is provided for the operation mode of the power grid, and the short-circuit current of the power grid is guaranteed not to be out of limits.
Owner:STATE GRID CORP OF CHINA +1

A method for rapid detection of microcystin in water

The invention discloses a method for quickly detecting microcystins in water. The method comprises the following steps: 1, filtering an obtained water sample, enriching and purifying the water samplewith a transition metal sulfide nano-material, and quickly passing the water through a filter, adjusting pH of the water sample to 1-5, and finally performing elution with pure water and methanol; 2,analyzing and determining the treated water sample with ultra-high performance liquid chromatography-tandem mass spectrometry. After the water sample is enriched and purified by the transition metal sulfide nanomaterial, MC-LR and MC-RR sensitivity can reach 20 ng / L and 10 ng / L respectively through cooperation with the ultra-high performance liquid chromatography- tandem mass spectrometry, the whole process time is shorter than 20 min, and dual requirements of the environmental monitoring department for timeliness and accuracy of microcystin detection can be fully met. Standard addition experiments prove that the recovery range of drinking water samples with the method reaches 97%-105%, and the recovery rate for waste water samples reaches 83%-99%, and the relative standard deviation is smaller than 5%. The method has the characteristics of high sensitivity, high analysis speed, high selectivity, simple operation and the like.
Owner:浙江中一检测研究院股份有限公司

Two-dimensional liquid chromatography-mass spectrometry method for mass analysis of low-molecular-weight heparin

The invention discloses a two-dimensional liquid chromatography-mass spectrometry method for mass analysis of low-molecular-weight heparin, which comprises the following steps: 1) preparing and grading low-molecular-weight heparin as a raw material through medium-pressure column chromatography to obtain a plurality of low-molecular-weight heparin oligosaccharides with different polymerization degrees, and 2) qualitatively analyzing the low-molecular-weight heparin oligosaccharide by using a two-dimensional liquid phase on-line mass spectrometry, namely separating the low-molecular-weight heparin oligosaccharide with a single polymerization degree by using strong anion exchange chromatography in a first-dimensional liquid phase, cutting each SAX separation oligosaccharide peak into a second-dimensional molecular sieve chromatography, and finally, carrying out on-line mass spectrometry. And 3) comparing SAX standard maps of different samples under the same polymerization degree, and carrying out semi-quantitative analysis on oligosaccharides of each polymerization degree through peak areas. The method can be used for quickly and finely analyzing the structure and controlling the quality of the low-molecular-weight heparin, and has huge application potential.
Owner:SUZHOU UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products