Device and method for analyzing Sr-90 in reactor decommissioned stainless steel material
A technology of analysis device and analysis method, which is applied to measurement devices, instruments, scientific instruments, etc., can solve the problems of cumbersome measurement and high price, and achieve the effects of good system stability, high recovery rate, simplified and controllable analysis process
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[0062] Take about 1g of the stainless steel (cast iron) sample contained in the heavy concrete of a certain reactor, add 1mg to 2mg of yttrium carrier, dissolve it in aqua regia, add hydrogen fluoride (analytical pure) and dissolve it again so that the sample to be analyzed is completely dissolved, and then evaporate the solution To nearly dry, use 3M HCl to dissolve to form a solution to obtain a spare solution, use a filter membrane with a pore size of 0.25 μm to filter, and after filtration, set the volume to 30 ml for use to obtain a solution to be separated. Connect one 2ml DGA resin (separation column Ⅰ) sequentially to the negative pressure vacuum box, use 10ml of 3M HCl solution to pre-balance the separation column Ⅰ in advance, and then separate the solution to be separated on the separation column Ⅰ, using 3M HCl and 0.1M HNO respectively 3 Rinse the separation column I to elute the interfering impurity elements Co, Ag, Cs, Fe, Ni, and finally use 0.1M HCl to elute th...
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