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A traditional Chinese medicine compound anti-virus multifunctional degradable polylactic acid fiber and its preparation method

A polylactic acid fiber, anti-virus technology, applied in the direction of fiber chemical characteristics, rayon manufacturing, single-component polyester rayon, etc., can solve the problem of increasing process steps and energy consumption, difficult mixing and uniform dispersion of fiber slices, and functional nano Particle effects cannot be effectively brought into play and other problems, to achieve good mixing and dispersing effects, simplify the preparation process, and good stability

Active Publication Date: 2021-08-17
芯安健康科技广东有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The problems of this process are: 1. The polymer fiber material first needs to be polymerized, separated, and processed into fiber slices, and then the fiber slices and functional nanoparticles are melt-mixed and extruded. The fiber slices have undergone two molding processes, which significantly increases process steps and energy consumption
2. It is difficult to mix and disperse the formed fiber slices evenly in the process of melting and mixing with functional nanoparticles, so that the effect of functional nanoparticles cannot be effectively exerted

Method used

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  • A traditional Chinese medicine compound anti-virus multifunctional degradable polylactic acid fiber and its preparation method
  • A traditional Chinese medicine compound anti-virus multifunctional degradable polylactic acid fiber and its preparation method

Examples

Experimental program
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Effect test

Embodiment 1

[0038] The preparation method of a traditional Chinese medicine composite anti-virus, anti-bacterial, anti-mite, far-infrared multifunctional degradable polylactic acid fiber includes the following preparation steps:

[0039] (1) Fermentation and extraction of corn to obtain lactic acid, and then dehydration condensation at a temperature of 100-170°C and reduced pressure to obtain a lactic acid prepolymer;

[0040] (2) Add 95 parts by mass of lactic acid prepolymer and 5 parts by mass of traditional Chinese medicine composite antiviral, antibacterial, anti-mite far-infrared multifunctional nanoparticles and catalyst stannous octoate into a twin-screw extruder, and melt and mix at a temperature of 160-200°C polycondensation to obtain functional polylactic acid;

[0041] (3) The obtained functional polylactic acid is formed by spinning to obtain a traditional Chinese medicine compound anti-virus, anti-bacterial, anti-mite and far-infrared multifunctional degradable polylactic ac...

Embodiment 2

[0048] The preparation method of a kind of traditional Chinese medicine compound anti-virus, anti-bacterial, anti-mite, far-infrared anion multifunctional degradable polylactic acid fiber of this embodiment includes the following preparation steps:

[0049] (1) Fermentation and extraction of corn to obtain lactic acid, and then dehydration condensation at a temperature of 100-170°C and reduced pressure to obtain a lactic acid prepolymer;

[0050] (2) Add 85 parts by mass of lactic acid prepolymer and 15 parts by mass of traditional Chinese medicine composite antiviral, antibacterial, anti-mite, far-infrared negative ion multifunctional nanoparticles and catalyst stannous octoate into a twin-screw extruder, and melt at a temperature of 160-200°C Mix polycondensation to obtain functional polylactic acid;

[0051] (3) The obtained functional polylactic acid is formed by spinning to obtain a traditional Chinese medicine compound anti-virus, anti-bacterial, anti-mite and far-infrar...

Embodiment 3

[0058] The preparation method of a kind of traditional Chinese medicine composite anti-virus, anti-bacterial, anti-mite anion anion multifunctional degradable polylactic acid fiber of this embodiment comprises the following preparation steps:

[0059] (1) Fermentation and extraction of corn to obtain lactic acid, and then dehydration condensation at a temperature of 100-170°C and reduced pressure to obtain a lactic acid prepolymer;

[0060] (2) Add 90 parts by mass of lactic acid prepolymer and 10 parts by mass of traditional Chinese medicine composite antiviral, antibacterial, anti-mite anion multifunctional nanoparticles and catalyst stannous octoate into a twin-screw extruder, melt, mix and polycondense at a temperature of 160-200°C , to obtain functional polylactic acid;

[0061] (3) The obtained functional polylactic acid is formed by spinning to obtain a traditional Chinese medicine compound anti-virus, anti-bacterial, anti-mite and far-infrared multifunctional degradabl...

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Abstract

The invention belongs to the field of functional fiber materials, and discloses a traditional Chinese medicine composite anti-virus multifunctional degradable polylactic acid fiber and a preparation method thereof. The starch fermentation raw material is fermented and extracted to obtain lactic acid, and then dehydrated and condensed to obtain a lactic acid prepolymer, and then added to an extruder with functional nanoparticles and a catalyst to melt, mix and polycondense to obtain functional polylactic acid, which is then spun and formed to obtain a product. The functional nanoparticles are obtained by absorbing the antiviral components of traditional Chinese medicine by adopting porous silicon dioxide and inorganic nanometer powder materials surface-modified by a silane coupling agent. The invention effectively couples the functional modification of the polylactic acid fiber with the upstream fiber polymerization, significantly simplifies the process steps and reduces production energy consumption, and has better mixing and dispersing effect and stability. At the same time, the inorganic antibacterial health function and the antiviral function of traditional Chinese medicine are integrated into the same particle, which can simultaneously exert antibacterial, antiviral and health care functions. The obtained functional fiber has the advantages of environmental protection, degradability and recycling.

Description

technical field [0001] The invention belongs to the field of functional fiber materials, and in particular relates to a traditional Chinese medicine composite anti-virus multifunctional degradable polylactic acid fiber and a preparation method thereof. Background technique [0002] Polylactic acid fiber is made from starch-containing agricultural products such as corn, wheat, and sugar beet. After fermentation to generate lactic acid, it is made by polycondensation and melt spinning. . Polylactic acid fiber is a kind of synthetic fiber whose raw material can be planted, is easy to plant, and the waste can be degraded naturally in nature. It can be decomposed into carbon dioxide and water by microorganisms in soil or seawater. When burned, it will not emit poisonous gas and cause pollution. It is a sustainable ecological fiber. The fabric has good handle and drapability, anti-ultraviolet radiation, low flammability and excellent processing performance. It is suitable for var...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F6/92D01F1/10
CPCD01F1/10D01F1/103D01F6/92
Inventor 黄钊维邓细利罗湘军钟敏丽黄蕊烨
Owner 芯安健康科技广东有限公司
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