Collecting device for corpse-derived odorant and detection and visual analysis method of corpse-derived odorant
An analysis method and collection device technology, applied in the field of forensic entomology, can solve the problems of complex corpses, lack of convenient collection, storage and analysis methods, destruction, etc., and achieve the effect of simple collection device, reduced detection cost, and short collection time
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1 Collection and preservation of corpse volatiles
1.1 Pretreatment of experimental materials
Experimental materials include:
Adsorption tube: Tenax Ta tube (6*150mm) was activated before use, treated with nitrogen blower at 300°C and constant helium flow (200ml / min) for 0.5 hours, then wrapped the port with parafilm and wrapped with tin foil Store at 4-8℃;
Beijing Labor Insurance Institute air sampler × 1; multi-section Teflon hose; body bag × 1; n-hexane; 2ml brown chromatography bottle; micropipette × 1; parafilm; tin foil.
[0026] 1.2 Installation and precautions
Insert the adsorption tube with one end of the Teflon hose into the body bag containing the corpse 10cm, make sure that the adsorption tube does not touch the corpse or the body bag. Place the air sampler in an upright position.
[0027] 1.3 Volatile adsorption
Three groups of odors were repeatedly collected from the same corpse, and the three groups were collected and mixed. At the same time, accordin...
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