Aqueous cathodic electrophoresis paint componsistion and its preparation method
A cathodic electrophoretic coating and composition technology, applied in the direction of electrophoretic coatings, etc., can solve the problems of insufficient durability and achieve the effects of reduced paint consumption, excellent electrodeposition stability and storage stability, and good throwing power
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[0042] 1. Synthesis of Isocyanate Blockers
[0043] name
regulations
grid
Dosage
(kg)
4.4-Diphenylmethane diisocyanate
Ester
work
industry
289.60
Diethylene glycol butyl ether
work
industry
220.40
work
industry
30.00
[0044] Process: Add isocyanate into a dry and clean reaction kettle equipped with a thermometer, agitator, reflux condenser and high level tank, and put diethylene glycol butyl ether into the high level tank. After stirring and raising the temperature to 45°C, start to add diethylene glycol butyl ether dropwise, control the temperature within the range of 45-60°C, finish the dropwise addition in 2 hours, add methyl isobutyl ketone, and then keep stirring for half an hour to confirm that the reaction is complete Finally, take a sample to measure the free NCO content, control the NCO value at 40-8...
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