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Microchannel reactors and fabrication processes

a microchannel reactor and reactor technology, applied in chemical/physical/physical-chemical processes, chemical processing, organic chemistry, etc., can solve the problems of thus the cost of containing high-pressure fluids in welded microchannels, microchannel devices that cannot withstand normal or elevated operating pressures, and reducing the amount of material

Inactive Publication Date: 2013-02-14
VELOCYS CORPORATION
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The patent describes a new technology for microchannel devices that uses welding instead of bonding or brazing to secure the layers of the device to each other. This reduces costs and allows for larger manufacturing scales. The technology also includes the use of particulate materials, such as catalysts or heat transfer materials, within the microchannels. The patent also describes methods for removing and replacing the particulate materials. Overall, the technology provides a more cost-effective and efficient way to manufacture microchannel devices.

Problems solved by technology

It is believed that without bonding the entire exposed surfaces of the shim layers to one another, the microchannel device will not withstand normal or elevated operating pressures.
One of the problems addressed by the exemplary embodiments is reducing the amount of material and thus cost to contain high pressure fluids in welded microchannel reactors that are not internally sealed, such as by using bonding or brazing.
Additional problems addressed by the exemplary embodiments are: (a) the need to load solid particulate materials into multiple parallel and separate microchannels contained within a pressure vessel with sufficient uniformity to achieve desired packing density, without which the chemical processor may not achieve desired performance; (b) the need to provide a precise, repeatable catalyst loading process for multiple parallel and separate microchannels contained within a pressure vessel, (b) the need to need to unload solid particulate materials from multiple parallel microchannels contained within a pressure vessel in order to refresh the chemical processor with new materials; (c) the need to provide loading and unloading of solid materials using a densification apparatus that is placed within a pressure vessel and which enables loading of multiple parallel microchannels with sufficient uniformity; and, (d) the need to provide service to chemical processors located in the field at a plant or in a remote location by using a portable densification apparatus that is placed within a pressure vessel and which enables loading of solid materials with sufficient uniformity into multiple parallel microchannels contained within said pressure vessel.

Method used

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  • Microchannel reactors and fabrication processes
  • Microchannel reactors and fabrication processes
  • Microchannel reactors and fabrication processes

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exemplary embodiment 200

[0164]Referring to FIG. 27, in an alternate exemplary embodiment 200, either exemplary structure 100, 100′ may include a positive pressure structure 202. For purposes of exemplary depiction only, the exemplary structure 100 is shown in FIG. 27 with the positive pressure structure. This positive pressure structure 202 includes an inlet pipe 204 supplying a pressurized fluid to the interior of the cavities by way of a respective egress orifice through the covers 134. By way of example, and not limitation, the pressurized fluid may be in inert fluid such as nitrogen that is directed into the cavities at a pressure greater than the pressure within the reaction microchannels of the reaction subassemblies 14. In this manner, the pressurized fluid provides a positive pressure upon the exterior of the microchannel module 10. But in a circumstance where, for whatever reason, the pressure of the pressurized fluid is no longer at or above the pressure occurring within the reaction microchannel...

exemplary embodiment 400

[0172]Referring to FIGS. 33-37, a further exemplary microchannel unit operation 400 is cylindrical and provides coaxial coolant delivery and reactant delivery. More specifically, the cylindrical shape is the result of a series of microchannel coolant and reaction subassemblies 402, 404 that alternate in a circular arrangement. In this exemplary embodiment 400, the microchannel coolant subassemblies 402 each comprise a shim or laminae 408 with preformed channels 410 (the channels may be formed by etching) that is joined with a top plate 412. In exemplary form, the preformed channels 410 are linear and extend horizontally. In exemplary form, the coolant shim 408 comprises a rectangular piece having constant dimensions of a width of 24 inches, a length of 24 inches, and a variable thickness that changes to accommodate for the difference in circumference on the interior of the unit operation 400 and the exterior of the unit operation. Alternatively, the coolant shim 408 may comprise a r...

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Abstract

A microchannel reactor comprising: (a) a plurality of process microchannels having particulates packed along the length of the microchannels; (b) a plurality of heat transfer microchannels in thermal communication with the plurality of process microchannels; and, (c) a first retainer positioned at a first end of the plurality of process microchannels to inhibit the particulates from exiting the process microchannels via the first end.

Description

CROSS-REFERENCE TO RELATED APPLICATIONS[0001]The present application claims the benefit of U.S. Provisional Patent Application Ser. No. 61 / 509,469, entitled, “MICROCHANNEL REACTORS AND FABRICATION PROCESSES,” filed Jul. 19, 2011, the disclosure of which is hereby incorporated by reference.INTRODUCTION TO THE INVENTION[0002]The present disclosure is directed to conducting chemical processing applications in by manifolding streams to and from multiple parallel reactor modules and, more specifically, to conducting processing in multiple reactor modules within pressure containing assemblies which have been designed to facilitate maintenance, repair, and replacement of packed beds of solid materials. The present disclosure includes methods and devices particularly useful for construction and operation of multiple parallel chemical processing modules, each module comprising multiple distinct and separate process channels, such as microchannels, where each channel comprising packed beds of...

Claims

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Application Information

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IPC IPC(8): B01J19/00C07C1/04
CPCB01J19/0093B01J2219/00783B01J2219/00806B29C67/00B01J2219/00835B01J2219/00844B01J2219/00873B01J2219/00817B01J8/0015B01J8/16B01J8/18B01J8/1881B01L2200/0647B01L2400/0436C10G2/32C10G2/34B01J19/00B01J2219/00867B01J2219/00801B01J2219/00932
Inventor LUZENSKI, ROBERTSLANE, JEFFERYYUSCHAK, THOMASNEAGLE, PAULMARCHIANDO, MICHAELLIPSKI, ROY
Owner VELOCYS CORPORATION