The invention provides a high-activity silver
powder, a preparation method and application thereof, and relates to the field of
metal powder metallurgy. The preparation method of the present invention comprises the following steps: S1, preparing
silver nitrate solution and framework agent solution, mixing
silver nitrate solution and framework agent solution, diluting, and preparing a
silver nitrate solution system whose concentration is 0.1-1.0g / L; S2 1. Dissolving the
reducing agent, adding a pH
regulator to obtain a reducing solution, mixing the reducing solution with the silver
nitrate solution system obtained in step S1, stirring at a
slow speed, and reacting to generate silver grains; S3, adding the dispersion
inducer to the obtained silver
nitrate in step S2 In the
system, mix evenly; S4, prepare the silver
nitrate solution with a concentration of 50-250g / L, add it to the
system obtained in step 3 within a predetermined time, after the addition is completed, let the material stand still, and age; S5, cleaning step S4 The material obtained in the process is settled to obtain highly active silver
powder. The silver powder obtained by the method of the invention has hollow structure, large specific surface area, high
catalytic efficiency and easy
sedimentation and separation.