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Method for preparing irrigating solution with anti-tumor function

A lavage fluid, anti-tumor technology, applied in the direction of anti-tumor drugs, medical preparations containing active ingredients, pharmaceutical formulas, etc.

Inactive Publication Date: 2010-03-31
山西华尚汇商贸有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The present invention provides a preparation method of lavage fluid with anti-tumor function in order to solve the problem of extracting hematoxylin with specific effect in the prior art

Method used

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  • Method for preparing irrigating solution with anti-tumor function
  • Method for preparing irrigating solution with anti-tumor function
  • Method for preparing irrigating solution with anti-tumor function

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] Embodiment 1, a method for preparing a lavage fluid with anti-tumor function, the steps include,

[0048] 1. Weigh 1000 grams of pulverized hematoxylin, the raw material drug must determine the species and source, dry, and crush it into pieces with a diameter of 1-2 mm and a length of 1-3 cm.

[0049] 2. Add 3000 grams of purified water, soak at room temperature for 12-24 hours,

[0050] 3. Boil for 30 minutes to extract, then separate the extract; then add 2000 grams of purified water and boil for 30 minutes to extract, then separate the extract; add 2000 grams of purified water and boil for 30 minutes to extract, then separate Go out extracting liquid; Merge the extracting liquid that obtains three times, concentrate under reduced pressure to 1000 grams,

[0051] 4. Freeze the concentrated solution at -20°C, then take it out and let it melt naturally at room temperature, filter to remove the precipitate,

[0052] 5. The concentrated solution obtained in the above st...

Embodiment 2

[0055] Embodiment 2, a method for preparing a lavage fluid with anti-tumor function, the steps include,

[0056] 1. Weigh 1000 grams of pulverized hematoxylin, the raw material drug must determine the species and source, dry, and crush it into pieces with a diameter of 1-2 mm and a length of 1-3 cm.

[0057] 2. Add 4000 grams of purified water, soak at room temperature for 12-24 hours,

[0058] 3. Boil for 30 minutes to extract, then separate the extract; then add 3000 grams of purified water and boil for 30 minutes to extract, then separate the extract; add 3000 grams of purified water and boil for 30 minutes to extract, then separate Go out extracting liquid; Merge the extracting liquid that obtains three times, concentrate under reduced pressure to 1500 grams,

[0059] 4. Freeze the concentrated solution at -20°C, then take it out and let it melt naturally at room temperature, filter to remove the precipitate,

[0060] 5. The concentrated solution obtained in the above st...

Embodiment 3

[0063] Embodiment 3, a method for preparing a lavage fluid with anti-tumor function, the steps include,

[0064] 1. Weigh 1000 grams of pulverized hematoxylin, the raw material drug must determine the species and source, dry, and crush it into pieces with a diameter of 1-2 mm and a length of 1-3 cm.

[0065] 2. Add 3500 grams of purified water, soak at room temperature for 12-24 hours,

[0066] 3. Boil for 30 minutes to extract, then separate the extract; add 2500 grams of purified water and boil for 30 minutes to extract, then separate the extract; add 2500 grams of purified water and boil for 30 minutes to extract, then separate Go out extracting solution; Merge the extracting solution that obtains three times, concentrate under reduced pressure to 1200 grams,

[0067] 4. Freeze the concentrated solution at -20°C, then take it out and let it melt naturally at room temperature, filter to remove the precipitate,

[0068] 5. The concentrated solution obtained in the above ste...

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Abstract

The invention relates to a method for preparing a sappan wood extract, in particular to a method for preparing an irrigating solution with an anti-tumor function. The method solves the problems of extracting sappan woods with specific effects in the prior art. The method comprises the following steps: weighing a certain amount of crushed sappan wood, adding purified water which is 3 to 5 times ofthe crushed sappan wood into the crushed sappan wood, soaking the crushed sappan wood for 12 to 24 hours at the room temperature, boiling the mixture for 30 minutes and separating an extract; adding water into the crushed sappan wood again, boiling the mixture for 30 minutes, extracting the mixture, and separating the extract; adding the purified water into the crushed sappan wood again, boiling the mixture for 30 minutes, extracting the mixture, and separating the extract; and combining the three extracts, performing vacuum concentration on the combined extract until the amount is 12 to 16 percent of the total amount of the added water, freezing and icing the concentrated solution at a temperature of 20 DEG C below zero, taking the frozen and iced concentrated solution out to unfreeze theconcentrated solution naturally at the room temperature, filtering the unfrozen concentrated solution to remove deposits, heating and boiling the concentrated solution obtained in the previous step again, freezing and icing the concentrated solution at a temperature of 20 DEG C below zero, taking the frozen and iced concentrated solution out to unfreeze the concentrated solution naturally at theroom temperature, and filtering the unfrozen concentrated solution to remove the deposits. The obtained product has significant anti-tumor effect.

Description

technical field [0001] The invention relates to a preparation method of sumac extract, in particular to a preparation method of lavage fluid with anti-tumor function. Background technique [0002] Brief introduction of sumac, sumac is the dry heartwood of small trees or shrubs of legume family. It tastes sweet, salty and slightly pungent, enters the heart, liver and spleen, and can promote blood circulation, remove blood stasis and relieve swelling pain. Studies in recent years have shown that in addition to the traditional effects of sumac, it also has various effects such as immunosuppression, anti-transplant rejection, and lowering blood sugar. In the 1970s, Japanese scholars discovered that the water extract of hematoxylin had a strong inhibitory effect on tumor cells in vitro, and there were also reports in this regard in China. For example, the effect of hematoxylin on killing and inducing apoptosis of human bladder cancer T24 cells, "Tumor Research and Clinic", Volum...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/48A61P35/00A61K135/00
Inventor 王国平任连生张蕻
Owner 山西华尚汇商贸有限公司
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