A kind of production method of phenolic foam wall insulation material
A technology of thermal insulation material and phenolic foam, which is applied in the production field of phenolic foam wall insulation material, can solve the problems of reducing thermal insulation effect and the like, and achieves the effect of reducing water absorption rate, reducing water absorption rate and wide application.
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[0019] Example 1:
[0020] (1) Backup raw materials: 350kg phenol, 175kg industrial paraformaldehyde, 1.5kg sodium hydroxide, 5kg acrylamide, 60kg water;
[0021] (2) Put the phenol, sodium hydroxide and water prepared in step (1) into the reaction kettle, raise the temperature to 70-85°C, slowly add the industrial paraformaldehyde prepared in step (1), and complete the addition within 1 hour;
[0022] (3) Put the acrylamide prepared in step (1) into the reaction kettle, slowly raise the temperature to 95-110°C, and keep the temperature at 95-110°C for 30-90 minutes;
[0023] (4) Reduce the temperature in the reactor to 40°C, add 10kg of water, 5kg of epichlorohydrin, and 2kg of sodium hydroxide, increase the temperature to 50~70°C, and stir for 1 hour;
[0024] (5) Reduce the temperature in the reactor to 40°C, slowly add 1kg of formic acid to the reactor while stirring to adjust the pH of the mixture in the reactor to neutral, and dehydrate 20kg to obtain epoxy modified phenolic resin...
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[0026] Example 2:
[0027] (1) Backup raw materials: 400kg phenol, 225kg industrial paraformaldehyde, 2kg sodium hydroxide, 25kg acrylamide, 120kg water;
[0028] Steps (2) to (3) are the same as in Example 1;
[0029] (4). Lower the temperature in the reactor to 40°C, add 60kg of water, 25kg of epichlorohydrin, and 10kg of sodium hydroxide, raise the temperature to 50~70°C, and stir for 6 hours;
[0030] (5) Reduce the temperature in the reactor to 40°C, slowly add 9kg of formic acid to the reactor while stirring to adjust the pH value of the mixture in the reactor to neutral, dehydrate 70kg to obtain epoxy modified phenolic resin;
[0031] (6) Take 40kg of epoxy-modified phenolic resin obtained in step (5), 1.3kg of silicone foam stabilizer, 2.5kg of n-pentane, and p-toluenesulfonic acid, benzenesulfonic acid, phosphoric acid, Dissolve 2.2kg of sulfuric acid in 0.5kg of water, mix and stir evenly, and then pour it into the preset mold. Use conventional methods to foam. The foaming de...
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