Method for detecting musk xylene in tobacco additive
A technology for xylene musk and tobacco additives, which is applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of public reports on the detection method of xylene musk in tobacco additives that have not been seen, and achieve high sensitivity and accurate determination methods Effect
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[0031] The present invention will be described in further detail below:
[0032] 1. Experimental part
[0033] 1.1 Instruments and reagents
[0034] Equipment: PE-Clarus600T gas-mass spectrometer (PE), HP-5MS (0.25μm×250μm×30m) chromatographic column (Agilent, USA), XP504 analytical balance (Mettler, Switzerland), SHZ-82 constant temperature oscillator ( Changzhou Guohua), SK5200H ultrasonic oscillator (Shanghai Kedao), LG10-2.4A high-speed centrifuge (Beijing Medical), separatory funnel, pipette, and other common laboratory glassware.
[0035] Reagents: cyclohexane, toluene, chloroform, D 15 -Musk xylene standard product, Musk xylene standard product, anhydrous sodium sulfate, ultrapure water (18.2MΩ resistivity).
[0036] 1.2 Preparation of standard solution
[0037] Weigh 0.1g (accurate to 0.001g) of the musk xylene standard substance in a 100mL volumetric flask, dissolve it with cyclohexane and dilute to the mark, prepare a 1mg / mL musk xylene standard stock solution, and store it at...
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