Elastomeric compositions that resist force loss
A technology of elastic components and copolymers, applied in bandages, absorbent pads, medical science, etc., can solve problems such as poor fit, performance loss, and increased discomfort
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example 1
[0227] Slow recovery stretch films were prepared using different amounts of elastomeric polymer, modified resin, and mineral oil as shown in Table 2. Blending was accomplished by extrusion of the blends (sample films F1a, F1b and F2) or by melt mixing in small batches and compression molding on a heated Carver press into films (sample films F3-F6). Sample films F1a and F1b comprise unhydrogenated styrene-isoprene-styrene (SIS) triblock copolymers, which are available under the trade name 4211 is commercially available from Dex Polymers L.P. (Houston, TX). Sample films F2 and F3 comprised hydrogenated styrene-ethylene-ethylene / propylene-styrene (SEEPS) triblock copolymers, which are available under the trade name Septon TM 4033 is commercially available from Kuraray America Inc. (Pasedena, TX). Sample films F4-F6 comprised a combination of SEEPS triblock copolymers available under the trade name Septon TM 4033 and Septon TM 4044 are commercially available from Kuraray Amer...
example 2
[0243] Slow recovery stretch laminates were prepared with the extruded films disclosed in Table 2 (sample films F1b and F2). Elastomeric film samples were cut about 40 millimeters wide by about 117 millimeters long for Sample Film Flb, or about 40 millimeters wide by about 147 millimeters long for Sample Film F2. Weigh the mass of each elastomer film to the nearest 0.1 mg. The basis weight (grams per square meter, "gsm") of each membrane was calculated by dividing the membrane weight (in grams) by the membrane area (length times width, in square meters). The slow recovery stretch laminates in Table 4 bonded multilayer laminate structures comprising two nonwovens sandwiching an elastomeric film. The nonwoven purchased from First Quality Nonwovens (Great Neck, NY) was a spunbond-meltblown-spunbond polypropylene thermally bonded nonwoven having a basis weight of about 22 gsm. A nonwoven was bonded to the first surface of the elastomeric film using a single layer of adhesive in ...
example 3
[0262] Example 3: Polymer Molecular Weight Determination
[0263] Polymer number average molecular weight and molecular weight distribution were determined by GPC SEC / MALS. GPC uses a Waters Alliance 2695HPLC autoinjector. It contains three Styragel HR columns (HR3, HR4 and HR5). The column heater was set to 30 °C. The flow rate was 1.0 mL / min and the mobile phase was HPLC grade tetrahydrofuran purchased from Sigma-Aldrich Inc. (St. Louis, MO). The detector was a Wyatt Dawn EOS light scattering detector calibrated with toluene, and 100 kilodalton polystyrene (molecular weight standards, purchased from Polysciences, Inc. (Warrington, PA)) and Waters 2414 refractive index were used in the mobile phase. Detectors were normalized at 30°C. Samples were prepared for analysis at a known concentration of 2 mg / mL. Samples were filtered using a 0.45 μm nylon membrane filter. The injection volume was 100 μL. Data were collected and analyzed using ASTRA 5.3.2.15. Values of dn / ...
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