Vibrating film and its preparation method and application
A vibrating membrane and metal technology, applied in the field of loudspeakers, can solve the problems of narrow frequency response range, affecting the pronunciation effect, lack of high-frequency vibrating membrane, etc.
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[0087] Preparation method of vibrating membrane
[0088] The invention also provides a preparation method of the vibrating film of the invention. Typically, this method includes:
[0089] Provide metal substrate;
[0090] Generating a metal oxide layer on at least one main surface of the metal substrate to obtain the vibrating film, specifically, a preferred method for preparing the vibrating film, comprising the following steps:
[0091] Carry out surface pretreatment on the metal substrate, successively carry out degreasing and derusting activation treatment in alkaline washing solution and pickling solution, then use ultrasonic cleaning in acetone solution, take it out and air dry;
[0092] An aqueous electrolyte solution containing fluoride ions is configured for anodic oxidation treatment;
[0093] In the aqueous electrolyte solution containing fluoride ions, the metal substrate is used as an anode, and the metal substrate is subjected to anodic oxidation treatment, th...
Embodiment 1
[0111] Diaphragm No.1
[0112] Next, the vibrating membrane is prepared with pure titanium as the metal substrate, including the following steps:
[0113] (1) Perform surface pretreatment on the pure titanium metal base material, successively wash in 5-20wt.% sodium hydroxide aqueous solution for 2-10 minutes, and the temperature of the sodium hydroxide washing solution is 40-150°C. After cleaning the metal substrate with clean water, put it into the pickling solution for cleaning for 2-10 minutes. The proportion of the pickling solution is hydrofluoric acid (10ml) + nitric acid (40ml) + deionized water (300ml). The acid-washed vibrating membrane was then ultrasonically cleaned in acetone solution, removed and air-dried.
[0114] (2) Prepare a 3wt.% phosphoric acid electrolyte aqueous solution for electrochemical anodic oxidation.
[0115] (3) Perform anodic oxidation treatment on the pure titanium metal substrate in an aqueous electrolyte solution, and the counter electrode...
Embodiment 2
[0119] Diaphragm No.2
[0120] Next, the vibrating membrane is prepared with pure titanium as the metal substrate, including the following steps:
[0121] (1) Perform surface pretreatment on the pure titanium metal base material, first wash in 5-20wt.% sodium hydroxide aqueous solution for 2-10 minutes, and the temperature of the alkaline washing solution is 40-150°C. After washing with water, put it into the pickling solution for 2-10 minutes. The proportion of the pickling solution is hydrofluoric acid (10ml) + nitric acid (40ml) + deionized water (300ml). The pure titanium metal substrate after pickling is then ultrasonically cleaned in acetone solution, taken out and air-dried.
[0122] (2) Configure the fluoride electrolyte for electrochemical anodic oxidation, NH in the electrolyte 4 The content of F is 0.25wt.%, the content of deionized water is 2wt.%, and the rest is ethylene glycol.
[0123](3) Perform anodic oxidation treatment on the pure titanium vibrating diaph...
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Abstract
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