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Polyacrylamide aqueous solution mine sampling viscosity stabilizer and its application method

A technology of polyacrylamide and viscosity stabilizer, which is applied in the field of sampling viscosity stabilizer of polyacrylamide aqueous solution and its application field, can solve the problems such as failure to reflect the real viscosity of polyacrylamide solution at the wellhead.

Inactive Publication Date: 2019-03-26
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When sampling the polyacrylamide solution in the polymer injection block, it was found that the viscosity of the sample was significantly lower than that of the solution prepared in the room, and the sampling did not reflect the true viscosity of the polyacrylamide solution at the wellhead

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] Preparation of polyacrylamide aqueous solution mine sampling viscosity stabilizer:

[0018] First take phenol: resorcinol = 3:0.5 mole parts to make mixed phenol, and then compound according to the ratio of bipyridine: mixed phenol: thiourea = 2:1.5: 0.5 mole parts to form polyacrylamide aqueous solution mine sampling viscosity stabilizer.

[0019] The use method of the polyacrylamide aqueous solution mine sampling viscosity stabilizer is carried out as follows:

[0020] a. Under the condition of nitrogen protection, take the polyacrylamide aqueous solution ore sampling viscosity stabilizer in a sealable sampling bottle of known volume, add deionized water to make an aqueous solution with a weight content of 28%, mix the sample The bottle is full of nitrogen, and then the bottle cap is sealed to obtain a polyacrylamide aqueous solution mine sampling viscosity stabilizer; or

[0021] Under the condition of nitrogen protection, use deionized water to mix bipyridyl, mixe...

Embodiment 2

[0026] Preparation of polyacrylamide aqueous solution mine sampling viscosity stabilizer:

[0027] First take phenol: resorcinol = 3:1.5 molar parts to make mixed phenol, and then compound it into polyacrylamide aqueous solution according to the ratio of bipyridine: mixed phenol: thiourea = 2:0.5: 1.5 molar parts. stabilizer.

[0028] The use method of the polyacrylamide aqueous solution mine sampling viscosity stabilizer is carried out as follows:

[0029] a. Under the condition of nitrogen protection, take the polyacrylamide aqueous solution ore sampling viscosity stabilizer in a sealable sampling bottle of known volume, add deionized water to make an aqueous solution with a weight content of 33%, mix the sample The bottle is full of nitrogen, and then the bottle cap is sealed to obtain a polyacrylamide aqueous solution mine sampling viscosity stabilizer; or

[0030] Under the condition of nitrogen protection, use deionized water to mix bipyridine, mixed phenol (mixed with...

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Abstract

The invention provides a polyacrylamide aqueous solution mine-field sampling viscosity stabilizing agent. The polyacrylamide aqueous solution mine-field sampling viscosity stabilizing agent is prepared from a Fe2+ ion complexing agent, a radical scavenger, and a deoxidant at a molar ratio of 2:0.5-1.5:0.5-1.5. The Fe2+ ion complexing agent is dipyridyl; the radical scavenger is a phenol mixture, and the phenol mixture is composed of phenol and resorcinol at a molar ratio of 3:0.5-1.5; and the deoxidant is thiourea. The polyacrylamide aqueous solution mine-field sampling viscosity stabilizing agent is capable of avoiding viscosity reduction of polyacrylamide aqueous solution in sampling processes caused by degradation; it is shown by comparing mine-field sampled polyacrylamide aqueous solution with in-door simulated polyacrylamide aqueous solution that mine-field sampling is capable of ensuring authenticity of sampling viscosity, and excellent application effect of mine-field sampling is achieved.

Description

technical field [0001] It is mainly used for sampling polyacrylamide solution in polymer injection block of oil field. Background technique [0002] At present, polymer flooding has become one of the effective ways to enhance oil recovery in the middle and later stages of development of integrated high water-cut oilfields. When sampling the polyacrylamide solution in the polymer injection block, it was found that the viscosity of the sample was significantly lower than that of the solution prepared in the room, and the sampling could not reflect the true viscosity of the polyacrylamide solution at the wellhead. Mines generally use clean water to prepare polyacrylamide mother liquor, and then mix it with sewage in the water injection pipeline in proportion and inject it into the well. The study found that because the sewage is in a closed and strongly reducing environment, iron ions form Fe 2+ It exists in the form of ions. When sampling, the polyacrylamide solution is expo...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N1/28G01N1/10
Inventor 汪庐山吕西辉张冬会张小卫薄纯辉田玉芹刘伟伟尹相文宋岱锋陈雷唐延彦陈伟江汇
Owner CHINA PETROLEUM & CHEM CORP
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