Hydrophobic modifying agent and method for preparing aerogel heat insulation felt from hydrophobic modifying agent

A hydrophobic modifier and aerogel technology are used in the field of hydrophobic modifiers and the preparation of aerogel thermal insulation felts with hydrophobic modifiers, which can solve the problem that aerogel thermal insulation blankets cannot be widely used and restrict aerogel thermal insulation. Felt manufacturing and development, increasing product cost and price, etc., to optimize the preparation of raw materials and processes, improve thermal insulation performance, and reduce production costs.

Active Publication Date: 2017-09-01
徐文忠 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, the modified raw materials used in the production of airgel insulation blankets are basically silane coupling agents, mainly trimethylchlorosilane, hexamethyldisilazane, 3-aminopropyltriethoxysilane and hexamethylsilane Such chemical substances are flammable and toxic to humans, and their emissions are restricted according to national environmental protection standards. This not only pollutes the environment, but also restricts the manufacture and development of airgel thermal insulation blankets, improving product quality. Cost and price, airgel insulation blanket has not been widely used so far

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Hydrophobic modifiers for airgel insulation blankets, including castor oil and oleic acid amide in a weight ratio of 6.8:3.2.

[0032] The method for preparing an airgel thermal insulation felt by using the above-mentioned hydrophobic modifier comprises the following steps:

[0033] Choose aluminum silicate fiber felt as insulation felt

[0034] (1) Prepare an airgel pre-fluid: after uniformly mixing the organosilicon solution and isopropanol according to a weight ratio of 1:1.3, adjust the pH to 4 with acetic acid, and prepare the airgel pre-fluid;

[0035] (2) Forming of the airgel composite thermal insulation blanket: the thermal insulation blanket is immersed in the airgel pre-fluid obtained in step (1), so that the thermal insulation blanket evenly absorbs the airgel pre-fluid to obtain the airgel composite Heat insulating felt, the weight ratio of described heat insulating felt and airgel pre-fluid is 1:2;

[0036] (3) Solvent replacement: place the airgel compo...

Embodiment 2

[0041] Hydrophobic modifiers for airgel insulation blankets, including castor oil and oleic acid amide in a weight ratio of 7.5:2.5.

[0042] The method for preparing an airgel thermal insulation felt by using the above-mentioned hydrophobic modifier comprises the following steps:

[0043] Choose glass fiber felt as insulation felt

[0044] (1) Prepare an airgel pre-fluid: after uniformly mixing the organosilicon solution and isopropanol according to a weight ratio of 1:1.8, adjust the pH to 3 with acetic acid to prepare the airgel pre-fluid;

[0045] (2) Forming of the airgel composite thermal insulation blanket: the thermal insulation blanket is immersed in the airgel pre-fluid obtained in step (1), so that the thermal insulation blanket evenly absorbs the airgel pre-fluid to obtain the airgel composite Heat insulating felt, the weight ratio of described heat insulating felt and airgel pre-fluid is 1:5;

[0046] (3) Solvent replacement: place the airgel composite thermal i...

Embodiment 3

[0051] Hydrophobic modifiers for airgel insulation blankets, including castor oil and oleic acid amide in a weight ratio of 7.2:2.8.

[0052] The method for preparing an airgel thermal insulation felt by using the above-mentioned hydrophobic modifier comprises the following steps:

[0053] Selecting Foamed Asbestos as Thermal Insulation Blanket

[0054] (1) Prepare the airgel pre-fluid: after uniformly mixing the organosilicon solution and isopropanol according to the weight ratio of 1:1.5, adjust the pH to 4 with acetic acid, and prepare the airgel pre-fluid;

[0055] (2) Forming of the airgel composite thermal insulation blanket: the thermal insulation blanket is immersed in the airgel pre-fluid obtained in step (1), so that the thermal insulation blanket evenly absorbs the airgel pre-fluid to obtain the airgel composite Heat insulation blanket, the weight ratio of described heat insulation blanket and airgel pre-fluid is 1:3;

[0056] (3) Solvent replacement: place the ai...

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PUM

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Abstract

The invention relates to a hydrophobic modifying agent, which comprises castor oil and oleamide according to a weight ratio of (6.8 to 7.5): (2.5 to 3.2). The material replaces a conventional silane coupling agent to be used as the hydrophobic modifying agent of the aerogel heat insulation felt. The use of dangerous chemicals and the pollution discharge are reduced, so that the production of the aerogel heat insulation felt achieves better environment-friendly effects, and is safe and economical. The method for preparing the aerogel heat insulation felt from the hydrophobic modifying agent comprises the steps of aerogel ahead fluid preparation, aerogel composite heat insulation felt forming, solvent replacement, modification, aging and drying. The preparation raw materials and the process are optimized; the raw material selection is safer and achieves a better environment-friendly effect; the operation process is simpler; the production period is greatly shortened; the production cost is greatly reduced; the heat insulation performance of the prepared aerogel heat insulation felt is further improved; the highest use temperature reaches 757 DEG C; the combustion grade reaches the grade A1; the heat conduction coefficient is lower than 7.715w / m.k.

Description

technical field [0001] The invention belongs to the technical field of thermal insulation materials, and relates to a hydrophobic modifier and a method for preparing an airgel thermal insulation blanket by using the hydrophobic modifier. Background technique [0002] At present, the modified raw materials used in the production of airgel insulation blankets are basically silane coupling agents, mainly trimethylchlorosilane, hexamethyldisilazane, 3-aminopropyltriethoxysilane and hexamethylsilane Such chemical substances are flammable and toxic to humans, and their emissions are restricted according to national environmental protection standards. This not only pollutes the environment, but also restricts the manufacture and development of airgel thermal insulation blankets, improving product quality. Due to cost and price, airgel thermal insulation blankets cannot be widely used so far. Contents of the invention [0003] According to the above problems, an object of the pre...

Claims

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Application Information

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IPC IPC(8): C04B30/02C04B38/08C04B41/47C04B111/27
CPCC04B30/02C04B41/009C04B41/472C04B2111/27C04B2201/32C04B14/06C04B14/4656C04B38/085C04B38/0074C04B38/0054C04B14/42C04B14/40C04B41/46C04B41/4535
Inventor徐文忠
Owner徐文忠