Sagger protective layer for producing vanadium nitrogen alloy and preparation method thereof
A technology of vanadium-nitrogen alloy and protective layer is applied in the field of vanadium-nitrogen alloy sintering device, which can solve the problem that the service life cannot be effectively extended in essence.
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Embodiment 1
[0030] The raw material analysis results are as follows: Mullite: Al 2 o 3 71.05wt%, SiO 2 26.41 wt%, true specific gravity 3.06, apparent porosity 3.35%, mullite phase 97.78wt%. Silicon carbide: SiC 97.90wt%.
[0031] Raw materials such as mullite, silicon carbide, sialon ceramic powder, metal aluminum powder, and metal silicon powder are sieved with a 200-mesh sieve, and the under-sieve is taken for later use. The above raw materials are 85wt% of mullite, 12wt% of silicon carbide, 2.0wt% of sialon ceramic powder, 0.5wt% of metal aluminum powder, and 0.5wt% of metal silicon powder according to the mass percentage of 100 kg. The solid powder material of the protective layer of the sintered box body is uniformly obtained. The organic solvent was obtained by mixing liquid phenolic resin and pure alcohol at a weight ratio of 90 wt%: 10 wt%. Add 50 kg of the prepared organic solvent to the above-mentioned 100 kg of prepared powder, stir evenly, and put it into a sealed plas...
Embodiment 2
[0034]The raw material analysis results are as follows: Mullite: Al 2 o 3 71.63wt%, SiO 2 26.05 wt%, true specific gravity 3.02, apparent porosity 3.38%, mullite phase 97.5wt%. Silicon carbide: SiC 97.0wt%.
[0035] Raw materials such as mullite, silicon carbide, sialon ceramic powder, metal aluminum powder, and metal silicon powder are sieved with a 200-mesh sieve, and the under-sieve is taken for later use. The above raw materials are 70wt% of mullite, 22wt% of silicon carbide, 5.0wt% of sialon ceramic powder, 1.5wt% of metal aluminum powder, and 1.5wt% of metal silicon powder according to the mass percentage of 100 kg. Mix and stir the prepared raw materials The solid powder material of the protective layer of the sintered box body is uniformly obtained. The organic solvent was prepared by mixing liquid phenolic resin and pure alcohol at a weight ratio of 80 wt%: 20 wt%. Add 40 kg of the prepared organic solvent to the above-mentioned 100 kg of prepared powder, stir ...
Embodiment 3
[0038] The raw material analysis results are as follows: Mullite: Al 2 o 3 71.55wt%, SiO 2 26.6 wt%, true specific gravity 3.03, apparent porosity 3.62%, mullite phase 97.53wt%. Silicon carbide: SiC 98.0wt%.
[0039] Raw materials such as mullite, silicon carbide, sialon ceramic powder, metal aluminum powder, and metal silicon powder are sieved with a 200-mesh sieve, and the under-sieve is taken for later use. The above raw materials are 75wt% of mullite, 18wt% of silicon carbide, 4.0wt% of sialon ceramic powder, 2.0wt% of metal aluminum powder, and 2.0wt% of metal silicon powder according to the mass percentage of 100 kg, and the prepared raw materials are mixed and stirred The solid powder material of the protective layer of the sintered box body is uniformly obtained. The organic solvent was obtained by mixing liquid phenolic resin and pure alcohol at a weight ratio of 70 wt%: 30 wt%. Add 30 kg of the prepared organic solvent to the above-mentioned 100 kg of prepared...
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