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Preparation method and application of red date and tobacco compounded Maillard reactant

A technology of Maillard reactant and jujube, which is applied in the fields of tobacco, application, and preparation of tobacco, can solve the problems of low purity, high irritation, and complex components of aroma components, and achieve strong tobacco aroma, improved smoke aroma, and The effect of simple operation steps

Active Publication Date: 2018-10-26
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, natural plant extracts and Maillard reaction products are used as tobacco flavors, and both have complex components, high content of macromolecular substances such as polysaccharides and proteins, many impurities, and low purity of biologically active substances such as aroma components, high viscosity, and high irritation. major defect

Method used

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  • Preparation method and application of red date and tobacco compounded Maillard reactant
  • Preparation method and application of red date and tobacco compounded Maillard reactant
  • Preparation method and application of red date and tobacco compounded Maillard reactant

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A preparation method of jujube tobacco compound Maillard reactant, comprising the steps of:

[0026] (1) Raw material pulverization: jujube pulp and tobacco raw materials are subjected to air-flow low-temperature ultrafine pulverization respectively to obtain jujube tobacco superfine powder, and the pulverization particle size is 40 μm;

[0027] (2) Low-temperature programmed pressurized Soxhlet extraction: put the jujube tobacco ultrafine powder into a microporous filter bag, add 5 times the mass of water, and perform low-temperature programmed pressurized Soxhlet cycle extraction once, and the filtrate is the red jujube tobacco extract ;

[0028] The said program pressurization condition is: 2min boost to 2bar, keep 10min, 2min boost to 4bar, keep 10min, 2min boost to 6bar, keep 10min, cycle 3 times;

[0029] (3) Biological fermentation, hydrolysis, transformation: add jujube tobacco extract and Portuguese clavisporalusitaniae (accounting for 1% of the mass of jujube...

Embodiment 2

[0033] A preparation method of jujube tobacco compound Maillard reactant, comprising the steps of:

[0034] (1) Raw material pulverization: Jujube pulp and tobacco raw materials are respectively subjected to air-flow low-temperature ultrafine pulverization to obtain jujube tobacco superfine powder, and the pulverization particle size is 30 μm;

[0035] (2) Low-temperature programmed pressurized Soxhlet extraction: put the jujube tobacco ultrafine powder into a microporous filter bag, add 10 times the mass of water, perform low-temperature programmed pressurized Soxhlet cycle extraction twice, and combine the filtrates to obtain red jujube tobacco extraction liquid;

[0036] The pressurized conditions of the program are as follows: boost the pressure to 3 bar in 3 minutes, keep it for 20 minutes, boost it to 5 bar in 3 minutes, keep it for 20 minutes, boost it to 7 bar in 3 minutes, keep it for 20 minutes, and cycle twice;

[0037] (3) Biological fermentation, hydrolysis, tran...

Embodiment 3

[0041] A preparation method of jujube tobacco compound Maillard reactant, comprising the steps of:

[0042] (1) Raw material pulverization: red jujube pulp and tobacco raw materials are subjected to air-flow low-temperature ultrafine pulverization respectively to obtain jujube tobacco superfine powder, and the pulverization particle size is 2 μm;

[0043] (2) Low-temperature programmed pressurized Soxhlet extraction: put the jujube tobacco ultrafine powder into a microporous filter bag, add 20 times the mass of water, perform low-temperature programmed pressurized Soxhlet cycle extraction once, and combine the filtrates to obtain jujube tobacco extraction liquid;

[0044] The pressurized conditions of the program are: boost to 4bar in 5 minutes, keep for 30min, boost to 6bar in 5min, keep for 30min, boost to 8bar in 5min, keep for 30min, and cycle once;

[0045] (3) Biological fermentation, hydrolysis, transformation: add jujube tobacco extract and Portuguese clavisporalusita...

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Abstract

The invention provides a preparation method of a red date and tobacco compounded Maillard reactant and application of the red date and tobacco compounded Maillard reactant. Red date pulp and discardedtobacco ultra-micro powder are put in a filter bag, low-temperature programmed pressurizing is conducted for Soxhlet extraction, a microbial strain is added into extraction liquid first for fermentation, then an enzyme is added for hydrolysis transformation, an auxiliary is added for suction filtration, macromolecule impurities are removed, the filtering efficiency is improved, amino acid and a catalyst are added for Maillard color enhancing and aroma enhancing reaction, and finally, concentration and freeze-drying are conducted to obtain the red date and tobacco Maillard reaction powder. Thered date and tobacco compounded Maillard reactant has few impurities and is high in purity and has harmonious, rich and natural aroma, the tobacco aroma is full and strong, the reactant has rich cocoa-coffee aroma, baking aroma, sweet aroma and the like, the spice quality is improved, and storage is easy. The invention further provides the application in traditional cigarettes and novel tobacco;the cigarette aroma is improved, soft and full, irritation is reduced, offensive odor is reduced, the appearance of cut tobacco has natural gloss, and the cut tobacco is close to high-quality cut tobacco; the technology conditions are mild, easy to implement and easy to operate.

Description

technical field [0001] The invention relates to the field of tobacco additives, in particular to a preparation method and application of jujube tobacco compound Maillard reactants. Background technique [0002] Tobacco additives are additives to improve the physical and chemical properties of tobacco, including flavor essences, humectants, combustion enhancers, anti-mold agents and adsorbents. The production of low-tar cigarettes needs more flavorings to make up for the lack of flavor. The purpose of tobacco product flavoring is to cover up the irritation and miscellaneous gas of natural tobacco, and to enhance or improve its fragrance. The spices used to prepare the liquid are generally less volatile. The spices used in the preparation of essences have different volatility. Those with high volatility are good for smelling, and others play the role of main fragrance and fixative fragrance (essence). Many aroma substances can be identified from tobacco and smoke. The syn...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B15/30A24B3/12
CPCA24B3/12A24B15/306C11B9/00C11B9/0003
Inventor 魏敏宋旭艳张耀华郭国宁周红审
Owner HUBEI CHINA TOBACCO IND
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