Flame-retardant wallpaper base material and preparation method thereof
A base material and flame retardant filler technology, applied in the field of wallpaper product manufacturing, can solve the problems of flexibility, tear strength reduction, poor appearance and hardening of wallpaper
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preparation example 1
[0029] Diatomaceous earth, carbon black, bamboo fiber, titanate, aluminate and silane coupling agent were stirred at 3000rpm for 4h and heated at 150°C for 2.5h according to the weight ratio of 100:10:1:3:3:50. , drying, cooling and grinding to obtain the modified diatomite;
[0030] Modified diatomite, graphene oxide, antimony trioxide, chitosan, brass powder, basalt fiber (1 μm), asbestos fiber (2 μm) and ceramic fiber (2 μm) according to 100:5:3:10: Mix at a weight ratio of 1:5:10:10. Under a nitrogen atmosphere, heat up from 20°C to 400°C at a rate of 5°C / min, and keep at 400°C for 1.5 hours; then, at a rate of 5°C / min The cooling rate is lowered to 70°C and cooled naturally; the flame-retardant filler for wallpaper is obtained, which is recorded as W1.
preparation example 2
[0032] Diatomaceous earth, carbon black, bamboo fiber, titanate, aluminate and silane coupling agent were stirred at 3500rpm for 5h at a weight ratio of 100:12:3:4:5:60, and heated at 165°C for 2h. drying, cooling and grinding to obtain the modified diatomite;
[0033] Modified diatomite, graphene oxide, antimony trioxide, chitosan, brass powder, basalt fiber (2 μm), asbestos fiber (2 μm) and ceramic fiber (1 μm) according to 100:6:5:12: Mix at a weight ratio of 3:10:12:13. Under a nitrogen atmosphere, heat up from 30°C to 450°C at a rate of 8°C / min, and keep at 450°C for 1 hour; then, cool down at a rate of 10°C / min Cool down to 60°C and then cool naturally; the flame-retardant filler for wallpaper is obtained, denoted as W2.
preparation example 3
[0035] Diatomaceous earth, carbon black, bamboo fiber, titanate, aluminate and silane coupling agent were stirred at 4000rpm for 4h and heated at 180°C for 0.5h according to the weight ratio of 100:15:5:5:7:80. drying, cooling and grinding to obtain the modified diatomite;
[0036] Modified diatomite, graphene oxide, antimony trioxide, chitosan, brass powder, basalt fiber (2 μm), asbestos fiber (1 μm) and ceramic fiber (1 μm) according to 100:8:8:15: Mix at a weight ratio of 5:15:15:15. Under a nitrogen atmosphere, heat up from 40°C to 500°C at a rate of 10°C / min, and keep at 500°C for 1 hour; then, cool down at a rate of 10°C / min. Cool down to 70°C and then cool naturally; the flame-retardant filler for wallpaper is obtained, denoted as W3.
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