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A kind of method for continuous liquefaction of high-concentration starch

A high-concentration, starch-based technology, which is applied in the field of starch sugar processing, can solve the problems of high-concentration starch milk gelatinization concentration, etc., and achieve the effect of less impurities, clear saccharification liquid and fast filtration speed

Active Publication Date: 2019-10-18
JILIN COFCO BIOCHEM +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It can be seen that this method does not effectively solve the problem of excessive concentration in the process of gelatinization and liquefaction of high-concentration starch milk.

Method used

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  • A kind of method for continuous liquefaction of high-concentration starch
  • A kind of method for continuous liquefaction of high-concentration starch
  • A kind of method for continuous liquefaction of high-concentration starch

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0080] (1) Using commercially available corn starch as a raw material, prepare a starch milk with a dry mass fraction of 45% by weight in a mixing tank at 50°C, and adjust the pH to 6.0 with 8M hydrochloric acid. Add 0.15‰ of medium temperature α-amylase, 0.2‰ of high temperature resistant α-amylase, 0.04‰ of lipase and 0.07‰ of neutral protease into the slurry tank, and keep the mixture at 55°C for 0.5h to obtain a brix value of 15 % Of the first starch milk;

[0081] (2) The first starch emulsion is discharged through a pipe for spray liquefaction, the temperature of the spray port is 108°C and the temperature is maintained in the pipe for 3 minutes, and the steam pressure is 0.6 MPa. The sprayed liquefied product is flashed, the temperature is lowered to 98°C, and then it is kept at 95°C for 2 hours to obtain a liquefied liquid.

[0082] After measurement, the DE value of the obtained liquefied liquid was 25, and the protein flocculated and floated on the liquefied liquid. Fil...

Embodiment 2

[0084] (1) Using commercially available corn starch as a raw material, prepare a starch milk with a dry mass fraction of 40% by weight in a mixing tank at 50°C, adjust the pH to 6.0 with 8M hydrochloric acid, and adjust the starch to the dry basis. Add 0.25‰ of medium temperature alpha-amylase, 0.2‰ of high temperature resistant alpha-amylase, 0.06‰ of lipase and 0.1‰ of neutral protease into the slurry tank. After mixing, keep it at 55°C for 1h to obtain a brix value of 15% 的 first starch milk;

[0085] (2) Stir and add corn starch to the first starch milk to obtain a second starch milk with a dry basis mass fraction of 55wt%, and add 0.25‰ of medium temperature α-amylase and 0.2‰ of the starch to the mixing tank. High-temperature resistant α-amylase, 0.06‰ lipase and 0.1‰ neutral protease are mixed and kept at 55°C for more than 0.5h to obtain a third starch milk with a brix value of 24%;

[0086] (3) With 0.18m 3 / h The third starch emulsion is discharged through the pipe for sp...

Embodiment 3

[0089] (1) Using commercially available corn starch as a raw material, prepare a starch milk with a dry mass fraction of 45% by weight in a mixing tank at 50°C, and adjust the pH to 6.0 with 8M hydrochloric acid. Add 0.35‰ of medium temperature α-amylase, 0.25‰ of high temperature resistant α-amylase, 0.08‰ of lipase, and 0.12‰ of neutral protease into the slurry tank, and keep the mixture at 55°C for 1.5h to obtain a brix value of 17 % Of the first starch milk;

[0090] (2) Stir and add corn starch to the first starch milk to obtain a second starch milk with a dry mass fraction of 70% by weight, and add 0.35‰ of medium temperature α-amylase and 0.25‰ of the blending tank to the mixing tank. High-temperature resistant α-amylase, 0.08‰ lipase and 0.12‰ neutral protease are mixed and kept at 55°C for more than 0.5h to obtain a third starch milk with a brix value of 22%;

[0091] (3) With 0.18m 3 / h The third starch emulsion is discharged through the pipe for spray liquefaction. The ...

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Abstract

The invention provides a method for continuously liquefying high-concentration corn starch with a jet liquefying technology. Medium-temperature amylase, high-temperature amylase, lipase and protease are combined for use, two-step pretreatment and continuous liquefying are preferably implemented, so that the viscosity of starch in a heating gelatinization process is reduced effectively, and high-concentration starch milk can be treated under lower steam jet pressure. According to the method, the dry matter content of a liquefying liquid can reach 40wt%-70wt%, the protein flocculation phenomenonis obvious after liquefying, and a saccharification liquid obtained after liquefying is high in filter speed and clear.

Description

Technical field [0001] The invention belongs to the technical field of starch sugar processing, and specifically relates to a method for liquefying high-concentration starch by direct heating and continuous injection of steam. Background technique [0002] Starch sugar is an important raw material for my country's food industry and a beneficial supplement for people's daily consumption of sugar. Therefore, it is particularly important to improve the quality of starch sugar products and reduce production costs. In recent years, the enzymatic hydrolysis sugar process has gradually replaced the acid sugar process. However, when the initial concentration of starch milk increases, the increase in starch paste viscosity makes it difficult to control liquefaction. Therefore, the current industry usually controls the initial concentration of starch milk at 25%-30%. However, the subsequent saccharification process requires evaporation to concentrate the saccharification liquid, so the lo...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C12P19/14C12P19/04
Inventor 佟毅刘安妮丁子元李义吴延东周哲曹雪陶进刘颖慰靳喜庆谭剑蔡菲
Owner JILIN COFCO BIOCHEM