Method for preparing high-performance silicon carbide coating on surface of carbon-carbon composite thermal insulation material

A technology of high-performance silicon carbide and thermal insulation materials, applied in the field of thermal insulation materials, can solve the problems of shortened life of carbon/carbon composite thermal insulation materials, wear and tear of thermal insulation materials, erosion of carbon/carbon composite thermal insulation materials, etc., to improve strength, combine The effect of firmness and service life improvement

Active Publication Date: 2019-05-31
ANHUI HONGCHANG NEW MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, some high-temperature industrial equipment (such as monocrystalline silicon growth furnaces, atmosphere sintering furnaces, etc.) mostly use inert gas for furnace temperature cooling, in which the particulate matter in the furnace will be mixed in the gas to form a high-speed particle flow, scouring the surface of the insulation material , so that the insulation material is subjected to a large amount of wear due to the erosion of the high-speed particle flow; in addition, there is a large amount of silicon vapor in the single crystal silicon growth furnace, which will react with the carbon / carbon composite insulation material at high temperature and gradually erode The carbon / carbon composite insulation material makes it invalid, and the existence of the above two factors will lead to a serious shortening of the life of the carbon / carbon composite insulation material

Method used

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A method for preparing a silicon carbide coating on the surface of a carbon / carbon composite thermal insulation material, comprising the following steps:

[0025] Step 1: The carbon / carbon composite thermal insulation material preform is made, and the initial density is customized to be 0.20g / cm according to the size of the required product 3 According to the designed product structure and size, the hard carbon felt is machined to the dimensional accuracy to obtain the carbon / carbon composite thermal insulation material blank;

[0026] Step 2: Pretreatment of the carbon / carbon composite thermal insulation material blank, the surface of the carbon / carbon composite thermal insulation material blank is polished, ultrasonically cleaned and then dried for use, the carbon / carbon composite thermal insulation material blank surface is polished, polished The sandpaper used for polishing is #600 sandpaper. Ultrasonic cleaning is carried out in absolute ethanol for 1 hour. After u...

Embodiment 2

[0034] A method for preparing a silicon carbide coating on the surface of a carbon / carbon composite thermal insulation material, comprising the following steps:

[0035] Step 1: The carbon / carbon composite thermal insulation material blank is made, and the initial density is customized to be 0.17g / cm according to the size of the required product 3 According to the designed product structure and size, the hard carbon felt is machined to the dimensional accuracy to obtain the carbon / carbon composite thermal insulation material blank;

[0036] Step 2: Pretreatment of the carbon / carbon composite thermal insulation material blank. The surface of the carbon / carbon composite thermal insulation material blank is polished, ultrasonically cleaned, and then dried for use. Grind and polish the surface of the carbon / carbon composite thermal insulation material blank. The sandpaper used for grinding and polishing is #600 sandpaper. Ultrasonic cleaning is carried out in absolute ethanol for ...

Embodiment 3

[0044] A method for preparing a silicon carbide coating on the surface of a carbon / carbon composite thermal insulation material, comprising the following steps:

[0045] Step 1: The carbon / carbon composite thermal insulation material preform is made, and the initial density is customized to be 0.18g / cm according to the size of the required product 3 According to the designed product structure and size, the hard carbon felt is machined to the dimensional accuracy to obtain the carbon / carbon composite thermal insulation material blank;

[0046] Step 2: Pretreatment of the carbon / carbon composite thermal insulation material blank. The surface of the carbon / carbon composite thermal insulation material blank is polished, ultrasonically cleaned, and then dried for use. Grind and polish the surface of the carbon / carbon composite thermal insulation material blank. The sandpaper used for grinding and polishing is #600 sandpaper. Ultrasonic cleaning is carried out in absolute ethanol fo...

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Abstract

The invention discloses a method for preparing a high-performance silicon carbide coating on the surface of a carbon-carbon composite thermal insulation material, and belongs to the technical field ofthermal insulation materials. The method comprises the following steps that a carbon / carbon composite thermal insulation material initial green body is prepared, rigid carbon felt with certain initial density is customized according to the size of a required product, the rigid carbon felt is machined to achieve the dimensional accuracy according to the designed product structure and size, and thecarbon / carbon composite thermal insulation material initial green body is obtained; the carbon / carbon composite thermal insulation material initial green body is pretreated, and the surface of the carbon / carbon composite thermal insulation material initial green body is subjected to grinding, polishing, ultrasonic cleaning and drying for use; coating slurry brushing is conducted, and ceramizationtreatment is conducted; deposited carbon treatment is conducted; high temperature sintering treatment is conducted. The silicon carbide coating prepared through the method is firmly bonded with a carbon / carbon composite thermal insulation material matrix, and the coating is not cracked, the strength of the surface coating of the carbon / carbon composite thermal insulation material is greatly improved, and the service life is obviously prolonged.

Description

technical field [0001] The invention relates to a method for preparing a high-performance silicon carbide coating on the surface of a carbon-carbon composite thermal insulation material, belonging to the technical field of thermal insulation materials. Background technique [0002] Carbon-carbon composite thermal insulation material is a carbon / carbon composite material composed of carbon fiber as a reinforcement and resin carbon or deposited carbon as a matrix. It is a new type of advanced thermal field material that can be used in high-temperature environments. Carbon-carbon composite thermal insulation The material has excellent properties such as low density, small linear expansion coefficient, high temperature resistance, strong thermal shock resistance, strong chemical corrosion resistance, high purity and no pollution. At the same time, there are a large number of micropores inside, resulting in small thermal conductivity and low heat capacity. Therefore, it has very ...

Claims

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Application Information

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Patent Type & AuthorityApplications(China)
IPC IPC(8): C04B35/83C04B35/622C04B41/87
CPCC04B35/622C04B35/83C04B41/87C04B41/009C04B41/5059C04B41/4517C04B41/4539C04B41/4554
Inventor蔡昌海肖孝天洪亮熊永祥宋良芬
OwnerANHUI HONGCHANG NEW MATERIAL CO LTD