Compound organic substance for efficiently removing vanadium from crude titanium tetrachloride and preparation method of the compound organic substance

A crude titanium tetrachloride and organic technology, applied in vanadium halide and other directions, can solve the problems of high reagent consumption, increased production cost, increased organic vanadium removal reagents, etc., to reduce industrial costs, reduce enterprise production costs, and reduce initial additions amount of effect
CN109956498AActive Publication Date: 2019-07-02BOHAI UNIV

Patent Information

Authority / Receiving Office
CN · China
Current Assignee / Owner
BOHAI UNIV
Publication Date
2019-07-02

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Abstract

The invention belongs to the field of purifying titanium tetrachloride with organic substances, and particularly relates to a compound organic substance for efficiently removing vanadium from crude titanium tetrachloride. The organic substance comprises: organic base oil, aromatic hydrocarbon oil, silicone oil, graphene and metal chloride, wherein the mass ratio of the components is (40-70):(2-10):(10-30):(5-10):(2-10), successively. The organic base oil is mixed white oil; the aromatic hydrocarbon oil is dimethylaniline; the silicone oil is dimethyl silicone oil; the graphene is copper-loadedgraphene oxide; the metal chloride is zinc chloride. The organic substance is easy to catalyze and crack, the vanadium removal efficiency is high, and the vanadium removal dosage is low.
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Description

technical field

[0001] The invention belongs to the field of refining titanium tetrachloride from organic matter, and in particular relates to a composite organic matter for efficient removal of vanadium from crude titanium tetrachloride and a preparation method thereof. Background technique

[0002] High-purity titanium is widely used in the aerospace field. The purity of titanium tetrachloride can directly affect the quality of titanium products for aviation. It is required that the content of pure titanium tetrachloride should reach 99.95%. In the process of refining titanium tetrachloride with organic matter, there is a problem of high addition of vanadium-removing reagents. The reason for this problem is mainly due to the slow cracking of organic matter, resulting in low carbon content involved in the reaction of vanadium removal, which affects the crude titanium refining process. removal efficiency. Therefore, in the process of refining titanium tetrachloride, it is n...

Claims

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